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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneSPB-5RTX-1HP-5MSDB-5
Column length (m) 30.60.60.30.30.
Carrier gas   HeHe 
Substrate      
Column diameter (mm) 0.250.320.220.250.25
Phase thickness (mum) 0.251.0.250.251.
Tstart (C) 60.40.60.60.50.
Tend (C) 270.230.230.280.290.
Heat rate (K/min) 15.3.2.4.10.
Initial hold (min)  2. 5.1.
Final hold (min) 15.10.35. 10.
I 1315.1309.1286.1305.1310.
ReferenceZaikin, 2010Engel and Ratel, 2007Paolini, Muselli, et al., 2007Saroglou, Marin, et al., 2007Bylaite and Meyer, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.40.
Tend (C) 220.280.280.285.300.
Heat rate (K/min) 5.3.4.4.34.
Initial hold (min) 10. 5. 5.
Final hold (min)      
I 1305.1305.1307.1301.1299.
ReferenceFlamini, Tebano, et al., 2006Kukic J., Petrovic S., et al., 2006Saroglou, Dorizas, et al., 2006Vujisic L., Vuckovic I., et al., 2006Vundac, Pfeifhofer, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSCP Sil 5 CBDB-5HP-5BPX-5
Column length (m) 30.25.30.30.25.
Carrier gas HeH2H2N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 80.80.35.60.50.
Tend (C) 300.270.270.220.300.
Heat rate (K/min) 4.10.5.5.5.
Initial hold (min)    10.5.
Final hold (min)   20.  
I 1307.91290.1310.1307.1319.
ReferenceZhao C.X., Li, et al., 2006Ziegenbein, Hanssen, et al., 2006Alves, Pinto, et al., 2005Celik, Gokturk, et al., 2005Dickschat J.S., Wagner-Dobler I., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase MDN-5HP-5DB-5HP-5HP-5MS
Column length (m) 30.30.25.30.30.
Carrier gas HeN2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.75.50.60.
Tend (C) 250.220.210.250.250.
Heat rate (K/min) 3.5.3.4.4.
Initial hold (min)  10.10.5.2.
Final hold (min)   1.15.20.
I 1305.1308.1306.1303.1306.
ReferenceDugo, Mondello, et al., 2005Flamini, Luigi Cioni, et al., 2005bin Jantan, Yalvema, et al., 2005Mahattanatawee, Goodner, et al., 2005Pino, Mesa, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5Mega 5MSHP-5MS
Column length (m) 60.25.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.20.20.250.25
Phase thickness (mum) 0.251.1.0.250.25
Tstart (C) 60.40.40.40.60.
Tend (C) 200.280.280.240.280.
Heat rate (K/min) 2.5.5.3.3.
Initial hold (min)    2. 
Final hold (min) 10.5.5.  
I 1305.1304.1304.1300.1305.
ReferenceSmadja, Rondeau, et al., 2005Solina, Baumgartner, et al., 2005Solina, Baumgartner, et al., 2005Verzera, Trozzi, et al., 2005Aligiannis, Kalpoutzakis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5SPB-5SPB-1SPB-1SPB-1
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 45.60.35.35.35.
Tend (C) 300.250.225.225.225.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min) 6.2.5.5.10.
Final hold (min) 10.20.20.20. 
I 1306.1306.1286.1286.1292.
ReferenceDugo, Mondello, et al., 2004Pino, Marbot, et al., 2004Chisholm, Jell, et al., 2003Chisholm, Jell, et al., 2003Chisholm, Wilson, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1HP-5DB-5HP-5
Column length (m) 25.25.30.30.30.
Carrier gas   N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.35.60.60.60.
Tend (C) 225.225.220.240.280.
Heat rate (K/min) 4.4.5.3.3.
Initial hold (min) 10.10.10.  
Final hold (min)      
I 1292.1288.1308.1307.1306.
ReferenceChisholm, Wilson, et al., 2003Chisholm, Wilson, et al., 2003Dural, Bagci, et al., 2003Flamini, Cioni, et al., 2003Fokialakis, Melliou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Mega 5MSDB-5BPX-5HP-5
Column length (m) 30.30.30.50.30.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.251.0.50.25
Tstart (C) 60.40.50.60.60.
Tend (C) 280.240.200.250.220.
Heat rate (K/min) 4.3.2.54.5.
Initial hold (min) 5.2. 5.10.
Final hold (min)    20. 
I 1305.1300.1308.81320.1308.
ReferenceSkaltsa, Demetzos, et al., 2003Verzera, Trozzi, et al., 2003Xu, van Stee, et al., 2003Bredie, Mottram, et al., 2002Flamini, Cioni, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 8 CBSPB-1BP-1BPX-5
Column length (m) 50.60.15.50.50.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.220.250.250.220.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.35.60.35.
Tend (C) 220.250.225.220.250.
Heat rate (K/min) 2.4.6.2.4.
Initial hold (min)  8.3. 3.
Final hold (min) 20.10.10. 10.
I 1288.1300.1292.1288.1316.
ReferenceLota, de Rocca Serra, et al., 2002Oruna-Concha, Ames, et al., 2002Chisholm, Wilson, et al., 2001Lota, Serra, et al., 2001Oruna-Concha, Duckham, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5CP Sil 8 CBHP-5HP-5
Column length (m) 30.50.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.251.050.250.250.25
Tstart (C) 60.50.40.50.50.
Tend (C) 280.290.280.280.280.
Heat rate (K/min) 4.2.4.4.4.
Initial hold (min) 5. 2.5.5.
Final hold (min)      
I 1305.1311.1311.1305.1305.
ReferenceSkaltsa, Mavrommati, et al., 2001David, Scanlan, et al., 2000Elmore, Mottram, et al., 2000Lazari, Skaltsa, et al., 2000Lazari, Skaltsa, et al., 2000, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5DB-5Mega 5MSMega 5MS
Column length (m) 10.30.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.10.250.250.250.25
Phase thickness (mum) 0.10.250.250.250.25
Tstart (C) 50.70.70.40.40.
Tend (C) 350.230.230.240.240.
Heat rate (K/min) 12.32.2.3.3.
Initial hold (min)    2.2.
Final hold (min)      
I 1311.1305.1305.1300.1300.
ReferenceMondello, Zappia, et al., 2000Song, Sawamura, et al., 2000Song, Sawamura, et al., 2000, 2Verzera, la Rosa, et al., 2000Verzera, Trozzi, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1OV-1OV-1DB-5
Column length (m) 30.50.20.20.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.220.320.320.32
Phase thickness (mum) 0.250.250.30.31.
Tstart (C) 50.60.45.45.40.
Tend (C) 280.230.220.220.210.
Heat rate (K/min) 4.2.10.10.3.
Initial hold (min) 5. 5.5. 
Final hold (min)  35.10.10. 
I 1305.1288.1290.1290.1310.
ReferenceLazari, Skaltsa, et al., 1999Lota, Serra, et al., 1999Valero, Sanz, et al., 1999Valero, Sanz, et al., 1999Moio and Addeo, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5SE-30DB-5DB-1
Column length (m) 30.60.50.30.60.
Carrier gas    H2 
Substrate      
Column diameter (mm) 0.250.330.320.320.25
Phase thickness (mum) 1.0.250.251.0.25
Tstart (C) -50.-50.50.40.35.
Tend (C) 180.180.250.220.280.
Heat rate (K/min) 6.6.4.3.2.
Initial hold (min)     10.
Final hold (min)     10.
I 1286.1309.1284.1310.1288.
ReferenceHelmig, Pollock, et al., 1996Helmig, Pollock, et al., 1996Misharina and Golovnya, 1996Moio L., Rillo L., et al., 1996Specht and Baltes, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101DB-1DB-1
Column length (m) 50.50.50.30.30.
Carrier gas N2N2He  
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum)   0.50  
Tstart (C) 80.80.50.50.50.
Tend (C) 200.200.250.300.300.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1287.1287.1278.1285.71285.9
ReferenceYang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Misharina, Aerove, et al., 1991Chang, Sheng, et al., 1989Chang, Sheng, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedPackedPacked
Active phase CP Sil 5 CBApiezon MApiezon MApiezon MSE-30
Column length (m) 25.1.51.51.5 
Carrier gas  N2N2N2 
Substrate  Celite 545Celite 545Celite 545Celite
Column diameter (mm) 0.22    
Phase thickness (mum)      
Tstart (C) 70.75.75.75.75.
Tend (C) 205.200.200.200.228.
Heat rate (K/min) 4.6.6.6. 
Initial hold (min)      
Final hold (min)      
I 1293.1272.1280.1281.1296.
ReferenceHendriks and Bruins, 1983Golovnya and Uraletz, 1971Golovnya and Uraletz, 1971Golovnya and Uraletz, 1971van den Dool and Kratz, 1963
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zaikin, 2010
Zaikin, V.G., Personal communication: Retention indices measured during 2010, 2010. [all data]

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Bylaite, E.; Meyer, A.S., · Characterisation of volatile aroma compounds of orange juices by three dynamic and static headspace gas chromatography techniques, Eur. Food Res. Technol., 2006, 222, 1-2, 176-184, https://doi.org/10.1007/s00217-005-0141-8 . [all data]

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Flamini, Cioni, et al., 2003
Flamini, G.; Cioni, P.L.; Morelli, I.; Ceccarini, L.; Andolfi, L.; Macchia, M., Composition of the essential oil of Medicago marina L. from the coastal dunes of Tuscany, Italy, Flavour Fragr. J., 2003, 18, 5, 460-462, https://doi.org/10.1002/ffj.1253 . [all data]

Fokialakis, Melliou, et al., 2003
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Skaltsa, Demetzos, et al., 2003
Skaltsa, H.D.; Demetzos, C.; Lazari, D.; Sokovic, M., Essential oil analysis and antimicrobial activity of eight Stachys species from Greece, Phytochemistry, 2003, 64, 3, 743-752, https://doi.org/10.1016/S0031-9422(03)00386-8 . [all data]

Verzera, Trozzi, et al., 2003
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References