1-Dodecene

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneDB-1DB-1SE-30SE-30
Column length (m)  10.10.40.40.
Carrier gas  HeHeH2H2
Substrate      
Column diameter (mm)  0.250.250.300.30
Phase thickness (μm)  0.250.25  
Temperature (C) 100.140.60.120.120.
I 1183.1188.1189.1189.1190.
ReferenceHeinzen, Soares, et al., 1999Beens, Tijssen, et al., 1998Beens, Tijssen, et al., 1998Gusev, Sokolov, et al., 1989Gusev, Sokolov, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedCapillaryCapillary
Active phase OV-101OV-1SE-30OV-1Squalane
Column length (m) 50.55.3.150. 
Carrier gas HeN2ArHe 
Substrate   Gas Chrom Q (80-100 mesh)  
Column diameter (mm) 0.250.21 0.50 
Phase thickness (μm)  0.35   
Temperature (C) 110.100.150.60.100.
I 1189.1187.91190.1194.1183.
ReferenceRang, Kuningas, et al., 1987Anders, Anders, et al., 1985Tiess, 1984Nijs and Jacobs, 1981Sojak, Hrivnak, et al., 1973
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneApiezon LSqualane
Column length (m)    45.200.
Carrier gas     H2
Substrate      
Column diameter (mm)    0.250.2
Phase thickness (μm)      
Temperature (C) 115.130.86.120.100.
I 1183.1184.1182.1190.11183.0
ReferenceSojak, Hrivnak, et al., 1973Sojak, Hrivnak, et al., 1973Sojak, Hrivnak, et al., 1973Eisen, Orav, et al., 1972Soják and Hrivnák, 1972
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualane
Column length (m) 200.200.200.
Carrier gas H2H2H2
Substrate    
Column diameter (mm) 0.20.20.2
Phase thickness (μm)    
Temperature (C) 115.130.86.
I 1183.41183.81182.5
ReferenceSoják and Hrivnák, 1972Soják and Hrivnák, 1972Soják and Hrivnák, 1972
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Heinzen, Soares, et al., 1999
Heinzen, V.E.F.; Soares, M.F.; Yunes, R.A., Semi-empirical topological method for the prediction of the chromatographic retention of cis- and trans-alkene isomers and alkanes, J. Chromatogr. A, 1999, 849, 2, 495-506, https://doi.org/10.1016/S0021-9673(99)00530-0 . [all data]

Beens, Tijssen, et al., 1998
Beens, J.; Tijssen, R.; Blomberg, J., Prediction of comprehensive two-dimensional gas chromatographic separations. A theoretical and practical exercise, J. Chromatogr. A, 1998, 822, 2, 233-251, https://doi.org/10.1016/S0021-9673(98)00649-9 . [all data]

Gusev, Sokolov, et al., 1989
Gusev, G.M.; Sokolov, V.P.; Yurov, V.V.; Kuznetsov, A.V.; Potatuev, A.A., Identification of olefins during hydrocarboxylation, Zh. Anal. Khim., 1989, 44, 551-555. [all data]

Rang, Kuningas, et al., 1987
Rang, S.; Kuningas, K.; Strenze, T.; Orav, A.; Eisen, O., Retention and Thermodynamics of Solution of n-Alkenes in OV-101, J. Chromatogr., 1987, 406, 75-80, https://doi.org/10.1016/S0021-9673(00)94018-4 . [all data]

Anders, Anders, et al., 1985
Anders, G.; Anders, K.; Engewald, W., Identification of non-branched alkenylcycloalkanes with a terminal double bond from retention index increments, Chromatographia, 1985, 20, 2, 83-86, https://doi.org/10.1007/BF02280602 . [all data]

Tiess, 1984
Tiess, D., Gaschromatographische Retentionsindices von 125 leicht- bis mittelflüchtigen organischen Substanzen toxikologisch-analytischer Relevanz auf SE-30, Wiss. Z. Wilhelm-Pieck-Univ. Rostock Math. Naturwiss. Reihe, 1984, 33, 6-9. [all data]

Nijs and Jacobs, 1981
Nijs, H.H.; Jacobs, P.A., On-Line Single Run Analysis of Effluents from a Fischer-Tropsch Reactor, J. Chromatogr. Sci., 1981, 19, 1, 40-45, https://doi.org/10.1093/chromsci/19.1.40 . [all data]

Sojak, Hrivnak, et al., 1973
Sojak, L.; Hrivnak, J.; Majer, P.; Janak, J., Capillary Gas Chromatography of Linear Alkenes on Squalane, Anal. Chem., 1973, 45, 2, 293-302, https://doi.org/10.1021/ac60324a039 . [all data]

Eisen, Orav, et al., 1972
Eisen, O.; Orav, A.; Rang, S., Identifizierung von Normal-Alkenen, Cyclopentenen und -Hexenen mittels Kapillar-Gas-Chromatographie. Identification des alcènes, cyclopentènes et -hexènes à l'aide de la chromatogrpahie en phase gazeuse sur colonne capillaire, Chromatographia, 1972, 5, 11, 229-239, https://doi.org/10.1007/BF02270600 . [all data]

Soják and Hrivnák, 1972
Soják, L.; Hrivnák, J., Open tubular column gas chromatography of the catalytic dehydrogenation products of n-dodecane, J. Chromatogr. Sci., 1972, 10, 11, 701-704, https://doi.org/10.1093/chromsci/10.11.701 . [all data]


Notes

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