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1-Tetradecene

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5 MSVF-5 MSUltra-ALLOY-5Ultra-ALLOY-5Ultra-ALLOY-5
Column length (m) 60.60.30.30.30.
Carrier gas HeliumHelium   
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 30.30.40.40.40.
Tend (C) 260.260.320.320.320.
Heat rate (K/min) 2.2.20.20.20.
Initial hold (min)   2.2.2.
Final hold (min) 28.28.13.13.13.
I 1392.1393.1392.1392.1394.
ReferenceLeffingwell and Alford, 2011Leffingwell and Alford, 2011Tsuge, Ohtan, et al., 2011Tsuge, Ohtan, et al., 2011Tsuge, Ohtan, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5DB-5Petrocol DHHP-5
Column length (m) 30.30.30.150.60.
Carrier gas HeliumNitrogenHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.251.00.25
Tstart (C) 70.40.60.40.30.
Tend (C) 290.230.260.300.260.
Heat rate (K/min) 5.2.4.1.2.
Initial hold (min)   4. 2.
Final hold (min) 10.   28.
I 1396.1389.1390.1390.1393.5
ReferenceRadulovic, Blagojevic, et al., 2010Scrivanti, Anton, et al., 2009Morteza-Semnani, Saeedi, et al., 2006Sojak, Kubinec, et al., 2006Leffingwell and Alford, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SE-54DB-5OV-1OV-101
Column length (m) 30.30.30.25.50.
Carrier gas HeliumHeHeH2N2
Substrate      
Column diameter (mm) 0.320.250.2490.310.25
Phase thickness (mum) 0.250.250.250.15 
Tstart (C) 40.60.60.70.80.
Tend (C) 250.260.300.220.200.
Heat rate (K/min) 5.2.3.3.2.
Initial hold (min) 2.5.   
Final hold (min) 5.    
I 1389.1391.1392.1388.1394.
ReferenceN/AKilic, Hafizoglu, et al., 2004Woerdenbag, Windono, et al., 2004Ramaroson-Raonizafinimanana, Gaydou, et al., 1997Tamura, Nakamoto, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101Cross-Linked MethylsiliconeDB-1DB-1Ultra-1
Column length (m) 50.25.30.30.25.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (mum)   0.250.250.25
Tstart (C) 80.35.50.50.80.
Tend (C) 200.225.240.240.260.
Heat rate (K/min) 2.4.5.5.3.
Initial hold (min)  3.3.3. 
Final hold (min)      
I 1395.1389.1396.1400.1389.
ReferenceTamura, Nakamoto, et al., 1995Bravo and Hotchkiss, 1993Shiota, 1993Shiota, 1993Okumura, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-101OV-101SP-2100
Column length (m) 60.60.50.50.30.
Carrier gas   NitrogenNitrogenHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum)      
Tstart (C) 50.50.70.80.40.
Tend (C) 230.230.200.200.250.
Heat rate (K/min) 4.4.2.2.4.
Initial hold (min)      
Final hold (min) 10.10.   
I 1389.1388.1395.1394.1389.
ReferenceBinder, Benson, et al., 1990Binder, Turner, et al., 1990Sugisawa, Nakamura, et al., 1990Sugisawa, Nakamura, et al., 1990Alencar, Alves, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase Apiezon L
Column length (m) 2.
Carrier gas  
Substrate Chromosorb G-AW-DMCS
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 25.
Tend (C)  
Heat rate (K/min) 10.
Initial hold (min)  
Final hold (min)  
I 1387.
ReferenceDahlmann, Köser, et al., 1979
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Leffingwell and Alford, 2011
Leffingwell, J.; Alford, E.D., Volatile constituents of the giant pufball mushroom (Calvatia gigantea), Leffingwell Rep., 2011, 4, 1-17. [all data]

Tsuge, Ohtan, et al., 2011
Tsuge, S.; Ohtan, H.; Watanabe, C., Pyrolysis - GC/MS Data Book of Synthetic Polymers, Elsevier, 2011, 420. [all data]

Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

Scrivanti, Anton, et al., 2009
Scrivanti, L.R.; Anton, A.M.; Zygadlo, J.A., Essential oil conposition of Bothriochloa Kuntze (Poaceae) from South America and their chemotaxonomy, Biochem. Systematics Ecol., 2009, 37, 3, 206-213, https://doi.org/10.1016/j.bse.2009.03.009 . [all data]

Morteza-Semnani, Saeedi, et al., 2006
Morteza-Semnani, K.; Saeedi, M.; Akbarsadeh, M.; Moshiri, K., The essential oil composition of Onosma microcarpum DC., Flavour Fragr. J., 2006, 21, 2, 314-316, https://doi.org/10.1002/ffj.1597 . [all data]

Sojak, Kubinec, et al., 2006
Sojak, L.; Kubinec, R.; Jurdakova, H.; Hajekova, E.; Bajus, M., GC-MS of polyethylene and polypropylene thermal cracking produxts, Petroleum Coal, 2006, 48, 1, 1-14. [all data]

Leffingwell and Alford, 2005
Leffingwell, J.C.; Alford, E.D., Volatile constituents of Perique tobacco, Electron. J. Environ. Agric. Food Chem., 2005, 4, 2, 899-915. [all data]

Kilic, Hafizoglu, et al., 2004
Kilic, A.; Hafizoglu, H.; Kollmannsberger, H.; Nitz, S., Volatile constituents and key odorants in leaves, buds, flowers, and fruits of Laurus nobilis L., J. Agric. Food Chem., 2004, 52, 6, 1601-1606, https://doi.org/10.1021/jf0306237 . [all data]

Woerdenbag, Windono, et al., 2004
Woerdenbag, H.J.; Windono, T.; Bos, R.; Riswan, S.; Quax, W.J., Composition of the essential oils of Kaempferia rotunda L. and Kaempferia angustifolia Roscoe rhizomes from Indonesia, Flavour Fragr. J., 2004, 19, 2, 145-148, https://doi.org/10.1002/ffj.1284 . [all data]

Ramaroson-Raonizafinimanana, Gaydou, et al., 1997
Ramaroson-Raonizafinimanana, B.; Gaydou, E.M.; Bombarda, I., Hydrocarbons from three vanilla bean species: V. fragrans, V. madagascariensis, and V. tahitensis, J. Agric. Food Chem., 1997, 45, 7, 2542-2545, https://doi.org/10.1021/jf960927b . [all data]

Tamura, Nakamoto, et al., 1995
Tamura, H.; Nakamoto, H.; Yang, R.-H.; Sugisawa, H., Characteristic aroma compounds in green algae (Ulva pertusa) volatiles, Nippon Shokuhin Kagaku Kogaku Kaishi, 1995, 42, 11, 887-891, https://doi.org/10.3136/nskkk.42.887 . [all data]

Bravo and Hotchkiss, 1993
Bravo, A.; Hotchkiss, J.H., Identification of volatile compounds resulting from the thermal oxidation of polyethylene, J. Appl. Polym. Sci., 1993, 47, 10, 1741-1748, https://doi.org/10.1002/app.1993.070471004 . [all data]

Shiota, 1993
Shiota, H., New esteric components in the volatiles of banana fruit (Musa sapientum L.), J. Agric. Food Chem., 1993, 41, 11, 2056-2062, https://doi.org/10.1021/jf00035a046 . [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]

Binder, Benson, et al., 1990
Binder, R.G.; Benson, M.E.; Flath, R.A., Volatile Components of Safflower, J. Agric. Food Chem., 1990, 38, 5, 1245-1248, https://doi.org/10.1021/jf00095a020 . [all data]

Binder, Turner, et al., 1990
Binder, R.G.; Turner, C.E.; Flath, R.A., Comparison of yellow starthistle volatiles from different plant parts, J. Agric. Food Chem., 1990, 38, 3, 764-767, https://doi.org/10.1021/jf00093a038 . [all data]

Sugisawa, Nakamura, et al., 1990
Sugisawa, H.; Nakamura, K.; Tamura, H., The aroma profile of the volatile in marine green algae (Ulva pertusa), Food Reviews International, 1990, 6, 4, 573-589, https://doi.org/10.1080/87559129009540893 . [all data]

Alencar, Alves, et al., 1983
Alencar, J.W.; Alves, P.B.; Craveiro, A.A., Pyrolysis of tropical vegetable oils, J. Agric. Food Chem., 1983, 31, 6, 1268-1270, https://doi.org/10.1021/jf00120a031 . [all data]

Dahlmann, Köser, et al., 1979
Dahlmann, G.; Köser, H.J.K.; Oelert, H.H., Multiple korrelation von retentionsindizes, Chromatographia, 1979, 12, 10, 665-671, https://doi.org/10.1007/BF02302943 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References