Hexane, 1-bromo-

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryPackedPackedPacked
Active phase HP-1HP-1ApolaneApiezon LApolane
Column length (m) 6.6.3.73.2.4
Carrier gas HeHe HeHe
Substrate    Chromosorb W AW DMCSChromosorb
Column diameter (mm) 0.3100.310   
Phase thickness (μm) 0.520.52   
Temperature (C) 20.20.130.75.70.
I 920.6921.4935.982.918.3
ReferenceKoutek, Cvacka, et al., 2001Koutek, Cvacka, et al., 2001Dutoit, 1991Castello and D'Amato, 1985Riedo, Fritz, et al., 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedPackedPacked
Active phase SqualaneApiezon LApiezon LSE-30Apiezon L
Column length (m) 100.2.32.33. 
Carrier gas  N2N2  
Substrate  DCMS-treated Chromosorb WDCMS-treated Chromosorb W Celite (40:60 Gewichtsverhaltnis)
Column diameter (mm) 0.25    
Phase thickness (μm)      
Temperature (C) 115.100.150.175.130.
I 918.942.960.948.951.
ReferenceLafosse and Thuaud-Chourrout, 1975Brown, Chapman, et al., 1968Brown, Chapman, et al., 1968Casteignau and Villessot, 1968von Kováts, 1958
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase Apiezon L
Column length (m)  
Carrier gas  
Substrate Celite (40:60 Gewichtsverhaltnis)
Column diameter (mm)  
Phase thickness (μm)  
Temperature (C) 190.
I 964.
Referencevon Kováts, 1958
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Koutek, Cvacka, et al., 2001
Koutek, B.; Cvacka, J.; Streinz, L.; Vrkocová, P.; Doubský, J.; Simonová, H.; Feltl, L.; Svoboda, V., Comparison of methods employing gas chromatography retention data to determine vapour pressures at 298 K, J. Chromatogr. A, 2001, 923, 1-2, 137-152, https://doi.org/10.1016/S0021-9673(01)00965-7 . [all data]

Dutoit, 1991
Dutoit, J., Gas chromatographic retention behaviour of some solutes on structurally similar polar and non-polar stationary phases, J. Chromatogr., 1991, 555, 1-2, 191-204, https://doi.org/10.1016/S0021-9673(01)87179-X . [all data]

Castello and D'Amato, 1985
Castello, G.; D'Amato, G., Gas Chromatography Separation and Identification of Linear and Branched-Chain Alkyl Bromides, J. Chromatogr., 1985, 324, 363-371, https://doi.org/10.1016/S0021-9673(01)81335-2 . [all data]

Riedo, Fritz, et al., 1976
Riedo, F.; Fritz, D.; Tarján, G.; Kováts, E.Sz., A tailor-made C87 hydrocarbon as a possible non-polar standard stationary phase for gas chromatography, J. Chromatogr., 1976, 126, 63-83, https://doi.org/10.1016/S0021-9673(01)84063-2 . [all data]

Lafosse and Thuaud-Chourrout, 1975
Lafosse, M.; Thuaud-Chourrout, N., Etude du comportement de composés halogénés et mèthoxylés en CG dans le cas de quatre phases stationnaires liquides pouvant former des liaisons de type donneur-accepteur d'électrons avec les groupes fonctionnels de ces composés, Chromatographia, 1975, 8, 4, 195-202, https://doi.org/10.1007/BF02274456 . [all data]

Brown, Chapman, et al., 1968
Brown, I.; Chapman, I.L.; Nicholson, G.J., Gas chromatography of polar solutes in electron acceptor stationary phases, Aust. J. Chem., 1968, 21, 5, 1125-1141, https://doi.org/10.1071/CH9681125 . [all data]

Casteignau and Villessot, 1968
Casteignau, G.; Villessot, D., Identification par chromatographie en phase gaseuse de composés difonctionnels insaturés. I. Synthèse et indices de rétention, Bull. Soc. Chim. Fr., 1968, 9, 3893-3903. [all data]

von Kováts, 1958
von Kováts, E., 206. Gas-chromatographische Charakterisierung organischer Verbindungen. Teil 1: Retentionsindices aliphatischer Halogenide, Alkohole, Aldehyde und Ketone, Helv. Chim. Acta, 1958, 41, 7, 1915-1932, https://doi.org/10.1002/hlca.19580410703 . [all data]


Notes

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