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Decanoic acid, methyl ester

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5HP-5MSRTX-5HP-5
Column length (m) 60.30.30.30.30.
Carrier gas  N2HeN2He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 1.0.250.250.250.25
Tstart (C) 40.60.60.40.50.
Tend (C) 230.220.280.300.250.
Heat rate (K/min) 3.5.4.5.4.
Initial hold (min) 2.10.5.2.5.
Final hold (min) 10.  10.15.
I 1324.1327.1325.1325.11328.
ReferenceEngel and Ratel, 2007Flamini, Tebano, et al., 2006Saroglou, Dorizas, et al., 2006Ádámová, Orinák, et al., 2005Mahattanatawee, Goodner, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSPB-5SPB-5SPB-5CP Sil 5 CB
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 250.250.250.250.280.
Heat rate (K/min) 4.4.4.4.3.
Initial hold (min) 2.2.2.2.10.
Final hold (min) 20.20.20.20.60.
I 1326.1326.1325.1325.1309.
ReferencePino, Mesa, et al., 2005Píno, Marbot, et al., 2004Pino, Marbot, et al., 2004Pino, Marbot, et al., 2004, 2Pino, Almora, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5SPB-5CP Sil 5 CBOV-1OV-1
Column length (m) 30.30.30.20.20.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.250.250.30.3
Tstart (C) 60.60.60.45.45.
Tend (C) 250.250.280.220.220.
Heat rate (K/min) 4.4.2.10.10.
Initial hold (min) 2.2.10.5.5.
Final hold (min) 20.20.40.10.10.
I 1324.1326.1306.1312.1310.
ReferencePino, Marbot, et al., 2003Pino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Valero, Sanz, et al., 1999Valero, Sanz, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-1Ultra-1SE-30
Column length (m) 50.30.30.50.22.
Carrier gas He H2H2N2
Substrate      
Column diameter (mm) 0.250.20.250.320.30
Phase thickness (mum) 0.250.250.250.521.0
Tstart (C) 140.50.35.35.60.
Tend (C)  300.259.259.250.
Heat rate (K/min) 8.5.2.2.2.
Initial hold (min)  2.   
Final hold (min)  5.   
I 1311.41307.1306.21306.61309.
ReferenceGolovnya, Syomina, et al., 1997Johnson, Urso, et al., 1997Farkas, Le Quere, et al., 1994Farkas, Le Quere, et al., 1994de Frutos, Sanz, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SP-2100SP-2100SP-2100SP-2100SP-2100
Column length (m)      
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Tstart (C) 170.170.170.170.170.
Tend (C)      
Heat rate (K/min) 2.4.6.2.4.
Initial hold (min)      
Final hold (min)      
I 1303.761309.671309.081320.621311.06
ReferencePodmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPacked
Active phase SP-2100CP Sil 5 CBDB-5SE-30
Column length (m)   30. 
Carrier gas H2H2He 
Substrate    Celite
Column diameter (mm)   0.26 
Phase thickness (mum)   0.25 
Tstart (C) 170.170.50.75.
Tend (C)   300.228.
Heat rate (K/min) 6.4.6. 
Initial hold (min)   4. 
Final hold (min)   20. 
I 1313.091306.481324.1310.
ReferencePodmaniczky, Szepesy, et al., 1986Podmaniczky, Szepesy, et al., 1986Rostad and Pereira, 1986van den Dool and Kratz, 1963
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Engel and Ratel, 2007
Engel, E.; Ratel, J., Correction of the data generated by mass spectrometry analyses of biological tissues: Application to food authentication, J. Chromatogr. A, 2007, 1154, 1-2, 331-341, https://doi.org/10.1016/j.chroma.2007.02.012 . [all data]

Flamini, Tebano, et al., 2006
Flamini, G.; Tebano, M.; Cioni, P.L.; Bagci, Y.; Dural, H.; Ertugrul, K.; Uysal, T.; Savran, A., A multivariate statistical approach to Centaurea classification using essential oil composition data of some species from Turkey, Pl. Syst. Evol., 2006, 261, 1-4, 217-228, https://doi.org/10.1007/s00606-006-0448-3 . [all data]

Saroglou, Dorizas, et al., 2006
Saroglou, V.; Dorizas, N.; Kypriotakis, Z.; Skaltsa, H.D., Analysis of the essential oil composition of eight Anthemis species from Greece, J. Chromatogr. A, 2006, 1104, 1-2, 313-322, https://doi.org/10.1016/j.chroma.2005.11.087 . [all data]

Ádámová, Orinák, et al., 2005
Ádámová, M.; Orinák, A.; Halás, L., Retention indices as identification tool in pyrolysis-capillary gas chromatography, J. Chromatogr. A, 2005, 1087, 1-2, 131-141, https://doi.org/10.1016/j.chroma.2005.01.003 . [all data]

Mahattanatawee, Goodner, et al., 2005
Mahattanatawee, K.; Goodner, K.L.; Baldwin, E.A., Volatile constituents and character impact compounds of selected Florida's tropical fruit, Proc. Fla. State Hort. Soc., 2005, 118, 414-418. [all data]

Pino, Mesa, et al., 2005
Pino, J.A.; Mesa, J.; Muñoz, Y.; Martí, M.P.; Marbot, R., Volatile components from mango (Mangifera indica L.) cultivars, J. Agric. Food Chem., 2005, 53, 6, 2213-2223, https://doi.org/10.1021/jf0402633 . [all data]

Píno, Marbot, et al., 2004
Píno, J.A.; Marbot, R.; Vázquez, C., Volatile components of the fruits of Vangueria madagascariensis J. F. Gmel. from Cuba, J. Essent. Oil Res., 2004, 16, 4, 302-304, https://doi.org/10.1080/10412905.2004.9698727 . [all data]

Pino, Marbot, et al., 2004
Pino, J.A.; Marbot, R.; Vazquez, C., Volatile components of tamarind (Tamarindus indica L.) grown in Cuba, J. Essent. Oil Res., 2004, 16, 4, 318-320, https://doi.org/10.1080/10412905.2004.9698731 . [all data]

Pino, Marbot, et al., 2004, 2
Pino, J.A.; Marbot, R.; Rosado, A.; Vázquez, C., Volatile constituents of Malay rose apple [Syzygium malaccense (L.) Merr. Perry], Flavour Fragr. J., 2004, 19, 1, 32-35, https://doi.org/10.1002/ffj.1269 . [all data]

Pino, Almora, et al., 2003
Pino, J.; Almora, K.; Marbot, R., Volatile components of papaya (Carica papaya L., maradol variety) fruit, Flavour Fragr. J., 2003, 18, 6, 492-496, https://doi.org/10.1002/ffj.1248 . [all data]

Pino, Marbot, et al., 2003
Pino, J.; Marbot, R.; Rosado, A.; Vázquez, C., Volatile constituents of fruits of Garcinia dulcis Kurz. from Cuba, Flavour Fragr. J., 2003, 18, 4, 271-274, https://doi.org/10.1002/ffj.1187 . [all data]

Pino, Marbot, et al., 2002
Pino, J.; Marbot, R.; Rosado, A., Volatile constituents of star apple (Chrysophyllum cainito L.) from Cuba, Flavour Fragr. J., 2002, 17, 5, 401-403, https://doi.org/10.1002/ffj.1116 . [all data]

Pino, Marbot, et al., 2002, 2
Pino, J.A.; Marbot, R.; Bello, A., Volatile compounds of Psidium salutare (H.B.K.) Berg. fruit, J. Agric. Food Chem., 2002, 50, 18, 5146-5148, https://doi.org/10.1021/jf0116303 . [all data]

Valero, Sanz, et al., 1999
Valero, E.; Sanz, J.; Martinez-Castro, I., Volatile components in microwave- and conventionally-heated milk, Food Chem., 1999, 66, 3, 333-338, https://doi.org/10.1016/S0308-8146(99)00069-2 . [all data]

Golovnya, Syomina, et al., 1997
Golovnya, R.V.; Syomina, L.A.; Samusenko, A.L., Nonlinear variation of sorption parameters of n-alkane homologs in temperature-programmed gas chromatography (TPGC) and new equation for calculation of retention indices, J. Hi. Res. Chromatogr., 1997, 20, 11, 611-614, https://doi.org/10.1002/jhrc.1240201108 . [all data]

Johnson, Urso, et al., 1997
Johnson, C.I.; Urso, A.; Geleta, L., Broad spectrum analysis of municipal and industrial effluents discharged into the Peace, Athabasca and Slave river basins: characterization of effluent samples, 1994 - Volume 1 of 2, Northern River Basins Study Project Report No. 121, Norther River Basins Study, Edmonton, Alberta, 1997, 27. [all data]

Farkas, Le Quere, et al., 1994
Farkas, P.; Le Quere, J.M.; Maarse, H.; Kovac, M., The standard GC retention index library of flavour compounds in Trends in flavour research. Proceedings of the 7th Weurman Flavour Research Symposium, Maarse,H.; van der Heij,D.G., ed(s)., Weurman Flavour Research Symposium, Noordwijkerhout, Netherlands, 1994, 145-149. [all data]

de Frutos, Sanz, et al., 1991
de Frutos, M.; Sanz, J.; Martinez-Castro, I., Characterization of artisanal cheeses by GC and GC/MS analysis of their medium volatility (SDE) fraction, J. Agric. Food Chem., 1991, 39, 3, 524-530, https://doi.org/10.1021/jf00003a019 . [all data]

Podmaniczky, Szepesy, et al., 1986
Podmaniczky, L.; Szepesy, L.; Lakszner, K.; Schomburg, G., Determination of Retention Indices in LPTGC, Chromatographia, 1986, 21, 7, 387-391, https://doi.org/10.1007/BF02346137 . [all data]

Rostad and Pereira, 1986
Rostad, C.E.; Pereira, W.E., Kovats and Lee retention indices determined by gas chromatography/mass spectrometry for organic compounds of environmental interest, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 6, 328-334, https://doi.org/10.1002/jhrc.1240090603 . [all data]

van den Dool and Kratz, 1963
van den Dool, H.; Kratz, P. Dec., A generalization of the retention index system including linear temperature programmed gas-liquid partition chromatography, J. Chromatogr., 1963, 11, 463-471, https://doi.org/10.1016/S0021-9673(01)80947-X . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References