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Thiophene

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PONAPONAPONAMethyl SiliconeDB-1
Column length (m) 50.50.50.60.60.
Carrier gas N2 Helium He
Substrate      
Column diameter (mm) 0.200.200.200.250.32
Phase thickness (mum) 0.500.500.500.251.0
Tstart (C) 35.30.30.40.40.
Tend (C) 170.150.170.220.280.
Heat rate (K/min) 2.2.2.5.2.
Initial hold (min)    10. 
Final hold (min)      
I 648.646.647.643.23685.
ReferenceYang, Wang, et al., 2004Yang, Wang, et al., 2003Yang, Yang, et al., 2003Baraldi, Rapparini, et al., 1999Tai and Ho, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5CP-Sil 5CP-Sil 5CP Sil 5 CB
Column length (m) 50.60.25.25.25.
Carrier gas  HeHeliumHeliumHe
Substrate      
Column diameter (mm) 0.220.250.320.320.32
Phase thickness (mum)   0.450.450.45
Tstart (C) 80.40.0.0.50.
Tend (C) 200.160.300.300.300.
Heat rate (K/min) 2.2.3.3.3.
Initial hold (min)  5.5.5. 
Final hold (min)      
I 650.677.644.645.644.
ReferenceEgolf and Jurs, 1993Macku and Shibamoto, 1991Damste, van Dalen, et al., 1988Damste, van Dalen, et al., 1988Damste, Kock-van Dalen, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase CP Sil 5 CB
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum) 0.45
Tstart (C) 50.
Tend (C) 300.
Heat rate (K/min) 3.
Initial hold (min)  
Final hold (min)  
I 645.
ReferenceDamste, Kock-van Dalen, et al., 1988
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Yang, Wang, et al., 2004
Yang, Y.; Wang, Z.; Zong, B.; Yang, H., Determination of sulfur compounds in fluid catalytic cracking gasoline by gas chromatography with a sulfur chemiluminiscence detector, Chin. J. Chromatogr., 2004, 22, 3, 216-219. [all data]

Yang, Wang, et al., 2003
Yang, Y.-T.; Wang, Z.; Han. J.-H.; Tian, H.-P.; Yang, H.-Y., Determination of sulfur compounds in gasoline fraction of microreactor products by gas chromatography - Atomic emission detector, Petrochemical Technology (Shiyou Huagong), 2003, 32, 11, 995-998. [all data]

Yang, Yang, et al., 2003
Yang, Y.T.; Yang, H.Y.; Zong, B.N.; Lu, W.Z., determination and distribution of sulfur compounds in gasoline by gas chromatography-atomic emission detector, Chinise J. Anal. Chem. (Fenxi Huaxue), 2003, 31, 10, 1153-1158. [all data]

Baraldi, Rapparini, et al., 1999
Baraldi, R.; Rapparini, F.; Rossi, F.; Latella, A.; Ciccioli, P., Volatile organic compound emissions from flowers of the most occurring and economically important species of fruit trees, Phys. Chem. Earth, 1999, 24, 6, 729-732, https://doi.org/10.1016/S1464-1909(99)00073-8 . [all data]

Tai and Ho, 1998
Tai, C.-Y.; Ho, C.-T., Influence of glutathione oxidation and pH on thermal formation of Maillard-type volatile compounds, J. Agric. Food Chem., 1998, 46, 6, 2260-2265, https://doi.org/10.1021/jf971111t . [all data]

Egolf and Jurs, 1993
Egolf, L.M.; Jurs, P.C., Quantitative structure-retention and structure-odor intensity relationships for a diverse group of odor-active compounds, Anal. Chem., 1993, 65, 21, 3119-3126, https://doi.org/10.1021/ac00069a027 . [all data]

Macku and Shibamoto, 1991
Macku, C.; Shibamoto, T., Volatile sulfur-containing compounds generated from the thermal interaction of corn oil and cysteine, J. Agric. Food Chem., 1991, 39, 11, 1987-1989, https://doi.org/10.1021/jf00011a021 . [all data]

Damste, van Dalen, et al., 1988
Damste, J.S.S.; van Dalen, A.C.K.; de Leeuw, J.W.; Schenck, P.A., Identification of homologous series of alkylated thiophenes, thiolanes, thianes and benzothiophenes present in pyrolisates of sulfur-rich kerogenes, J. Chromatogr., 1988, 435, 435-452, https://doi.org/10.1016/S0021-9673(01)82208-1 . [all data]

Damste, Kock-van Dalen, et al., 1988
Damste, J.S.S.; Kock-van Dalen, A.C.; de Leeuw, J.W.; Schenk, P.A., Identification of homologous series of alkylated thiophenes, thiolanes, thianes and benzothiophenes present in pyrolysates of sulphur-rich kerogens, J. Chromatogr., 1988, 435, 435-452, https://doi.org/10.1016/S0021-9673(01)82208-1 . [all data]


Notes

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