Thiophene, tetrahydro-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101PONAPONARSL-200OV-101
Column length (m) 25.50.50.30.50.
Carrier gas Helium HeliumH2 
Substrate      
Column diameter (mm) 0.200.200.200.250.22
Phase thickness (μm) 0.250.500.500.25 
Tstart (C) 70.30.30.40.80.
Tend (C) 200.150.170.280.200.
Heat rate (K/min) 3.2.2.6.2.
Initial hold (min) 2.  2. 
Final hold (min)    10. 
I 838.779.782.802.801.
ReferenceBlazevic and Mastelic, 2008Yang, Wang, et al., 2003Yang, Yang, et al., 2003Jirovetz, Smith, et al., 2002Egolf and Jurs, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5CP-Sil 5CP-Sil 5CP Sil 5 CBCP Sil 5 CB
Column length (m) 25.25.25.25.25.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.450.450.450.450.45
Tstart (C) 0.0.0.50.50.
Tend (C) 300.300.300.300.300.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min) 5.5.5.  
Final hold (min)      
I 775.775.778.775.775.
ReferenceDamste, van Dalen, et al., 1988Damste, van Dalen, et al., 1988Damste, van Dalen, et al., 1988Damste, Kock-van Dalen, et al., 1988Damste, Kock-van Dalen, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase CP Sil 5 CB
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (μm) 0.45
Tstart (C) 50.
Tend (C) 300.
Heat rate (K/min) 3.
Initial hold (min)  
Final hold (min)  
I 778.
ReferenceDamste, Kock-van Dalen, et al., 1988
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Blazevic and Mastelic, 2008
Blazevic, I.; Mastelic, J., Free and bounded volatiles of rocket (Eruca sativa Mill.), Fravour Fragr. J., 2008, 23, 4, 278-285, https://doi.org/10.1002/ffj.1883 . [all data]

Yang, Wang, et al., 2003
Yang, Y.-T.; Wang, Z.; Han. J.-H.; Tian, H.-P.; Yang, H.-Y., Determination of sulfur compounds in gasoline fraction of microreactor products by gas chromatography - Atomic emission detector, Petrochemical Technology (Shiyou Huagong), 2003, 32, 11, 995-998. [all data]

Yang, Yang, et al., 2003
Yang, Y.T.; Yang, H.Y.; Zong, B.N.; Lu, W.Z., determination and distribution of sulfur compounds in gasoline by gas chromatography-atomic emission detector, Chinise J. Anal. Chem. (Fenxi Huaxue), 2003, 31, 10, 1153-1158. [all data]

Jirovetz, Smith, et al., 2002
Jirovetz, L.; Smith, D.; Buchbauer, G., Aroma compound analysis of Eruca sativa (Brassicaceae) SPME headspace leaf samples using GC, GC-MS, and olfactometry, J. Agric. Food Chem., 2002, 50, 16, 4643-4646, https://doi.org/10.1021/jf020129n . [all data]

Egolf and Jurs, 1993
Egolf, L.M.; Jurs, P.C., Quantitative structure-retention and structure-odor intensity relationships for a diverse group of odor-active compounds, Anal. Chem., 1993, 65, 21, 3119-3126, https://doi.org/10.1021/ac00069a027 . [all data]

Damste, van Dalen, et al., 1988
Damste, J.S.S.; van Dalen, A.C.K.; de Leeuw, J.W.; Schenck, P.A., Identification of homologous series of alkylated thiophenes, thiolanes, thianes and benzothiophenes present in pyrolisates of sulfur-rich kerogenes, J. Chromatogr., 1988, 435, 435-452, https://doi.org/10.1016/S0021-9673(01)82208-1 . [all data]

Damste, Kock-van Dalen, et al., 1988
Damste, J.S.S.; Kock-van Dalen, A.C.; de Leeuw, J.W.; Schenk, P.A., Identification of homologous series of alkylated thiophenes, thiolanes, thianes and benzothiophenes present in pyrolysates of sulphur-rich kerogens, J. Chromatogr., 1988, 435, 435-452, https://doi.org/10.1016/S0021-9673(01)82208-1 . [all data]


Notes

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