Benzene, chloro-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Petrocol DHDB-1DB-5OV-1DB-5
Column length (m) 50.30.30. 30.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.250.25 0.53
Phase thickness (μm) 0.50.251. 1.5
Tstart (C) 35.40.50.35.50.
Tend (C) 200.325.200.300. 
Heat rate (K/min) 3.3.2.58.2.
Initial hold (min) 10.    
Final hold (min) 10.    
I 831.2821.2852.4826.5836.42
ReferenceCensullo, Jones, et al., 2003Sun and Stremple, 2003Xu, van Stee, et al., 2003Gautzsch and Zinn, 1996Gerbino, Garbarino, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-1DB-1
Column length (m) 30.30.30.30.30.
Carrier gas N2N2 N2N2
Substrate      
Column diameter (mm) 0.530.530.250.2350.235
Phase thickness (μm) 1.51.51.0.250.25
Tstart (C) 50.50.-50.50.50.
Tend (C)   180.  
Heat rate (K/min) 2.2.6.10.5.
Initial hold (min)    0.0.
Final hold (min)      
I 837.68840.15825.3833.830.
ReferenceGerbino, Garbarino, et al., 1996Gerbino, Garbarino, et al., 1996Helmig, Pollock, et al., 1996Gerbino and Castello, 1995Gerbino and Castello, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPacked
Active phase Petrocol DHSE-54SE-30
Column length (m) 100.25.3.05
Carrier gas HeH2He
Substrate   Chromosorb AW
Column diameter (mm) 0.250.31 
Phase thickness (μm) 0.50.17 
Tstart (C) 30.35.40.
Tend (C) 220. 210.
Heat rate (K/min) 1.2.10.
Initial hold (min)   10.
Final hold (min)   30.
I 825.852.839.
ReferenceWhite, Hackett, et al., 1992Weber, 1986Buchman, Cao, et al., 1984
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Censullo, Jones, et al., 2003
Censullo, A.C.; Jones, D.R.; Wills, M.T., Speciation of the volatile organic compounds (VOCs) in solventborne aerosol coatings by solid phase microextraction-gas chromatography, J. Coat. Technol., 2003, 75, 936, 47-53, https://doi.org/10.1007/BF02697922 . [all data]

Sun and Stremple, 2003
Sun, G.; Stremple, P., Retention index characterization of flavor, fragrance, and many other compounds on DB-1 and DB-XLB, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/pdf/b-0279.pdf. [all data]

Xu, van Stee, et al., 2003
Xu, X.; van Stee, L.L.P.; Williams, J.; Beens, J.; Adahchour, M.; Vreuls, R.J.J.; Brinkman, U.A.Th.; Lelieveld, J., Comprehensive two-dimensional gas chromatography (GC×GC) measurements of volatile organic compounds in the atmosphere, Atmos. Chem. Phys., 2003, 3, 3, 665-682, https://doi.org/10.5194/acp-3-665-2003 . [all data]

Gautzsch and Zinn, 1996
Gautzsch, R.; Zinn, P., Use of incremental models to estimate the retention indexes of aromatic compounds, Chromatographia, 1996, 43, 3/4, 163-176, https://doi.org/10.1007/BF02292946 . [all data]

Gerbino, Garbarino, et al., 1996
Gerbino, T.C.; Garbarino, G.; Petit-Bon, P., Programmed temperature retention indices: calculation of linear programmed temperature retention indices of halogenated benzenes from isothermal data, Ann. Chim. (Rome), 1996, 86, 63-75. [all data]

Helmig, Pollock, et al., 1996
Helmig, D.; Pollock, W.; Greenberg, J.; Zimmerman, P., Gas chromatography mass spectrometry analysis of volatile organic trace gases at Mauna Loa Observatory, Hawaii, J. Geophys. Res., 1996, 101, D9, 14697-14710, https://doi.org/10.1029/96JD00212 . [all data]

Gerbino and Castello, 1995
Gerbino, T.C.; Castello, G., Prediction of programmed temperature retention indices on capillary columns of different polarities, J. Chromatogr. A, 1995, 699, 1-2, 161-171, https://doi.org/10.1016/0021-9673(95)00024-H . [all data]

White, Hackett, et al., 1992
White, C.M.; Hackett, J.; Anderson, R.R.; Kail, S.; Spock, P.S., Linear temperature programmed retention indices of gasoline range hydrocarbons and chlorinated hydrocarbons on cross-linked polydimethylsiloxane, J. Hi. Res. Chromatogr., 1992, 15, 2, 105-120, https://doi.org/10.1002/jhrc.1240150211 . [all data]

Weber, 1986
Weber, L., Utilization of the Sadtler standard RI system in micropollution analyses, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 8, 446-451, https://doi.org/10.1002/jhrc.1240090806 . [all data]

Buchman, Cao, et al., 1984
Buchman, O.; Cao, G.-Y.; Peng, C.T., Structure assignment by retention index in gas-liquid radiochromatography of substituted cyclohexenes, J. Chromatogr., 1984, 312, 75-90, https://doi.org/10.1016/S0021-9673(01)92765-7 . [all data]


Notes

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