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Nordazepam

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type PackedCapillaryCapillaryPackedPacked
Active phase SE-30BP-1DB-5SE-30SE-30
Column length (m) 2. 15.2.2.
Carrier gas Nitrogen HeHeNitrogen
Substrate Chromosorb G AW DMCS (80-100 mesh)  Chromosorb W(100-120 mesh)Chromosorb W AW DMS (80-100 mesh)
Column diameter (mm)   0.25  
Phase thickness (mum)   0.25  
Tstart (C) 100.100.150.200.130.
Tend (C) 300.300.260.285.290.
Heat rate (K/min)   10.4.8.
Initial hold (min)   1.2.2.
Final hold (min)    10.8.
I 2496.2522.2522.2502.2480.
ReferenceMHA, 9999MHA, 9999Zamechnik, Ethier, et al., 1989Chiarotti, de Giovanni, et al., 1986Peel and Perrigo, 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase SE-30
Column length (m) 2.
Carrier gas N2
Substrate Chromosorb W AW DMS
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 130.
Tend (C) 290.
Heat rate (K/min) 8.
Initial hold (min) 2.
Final hold (min) 8.
I 2480.
ReferencePeel and Perrigo, 1975
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

MHA, 9999
MHA, Directorate of ForensicScience., Forensic Toxicology, 9999. [all data]

Zamechnik, Ethier, et al., 1989
Zamechnik, J.; Ethier, J.-C.; Neville, G.A., Benzodiazepines- an extensive collection of mass spectra, J. Can. Soc. Forensic Sci., 1989, 22, 3, 233-259, https://doi.org/10.1080/00085030.1989.10757437 . [all data]

Chiarotti, de Giovanni, et al., 1986
Chiarotti, M.; de Giovanni, N.; Fiori, A., Analysis of Benzodiazepines. I. Chromatographic Identification, J. Chromatogr., 1986, 358, 169-178, https://doi.org/10.1016/S0021-9673(01)90326-7 . [all data]

Peel and Perrigo, 1976
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can. Soc. Forens. Sci. J., 1976, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]

Peel and Perrigo, 1975
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can.Soc.Forens.Sci.J., 1975, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]


Notes

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