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2,6-Lutidine

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type PackedPackedPackedCapillaryCapillary
Active phase C78, Branched paraffinC78, Branched paraffinApolaneSE-30SE-30
Column length (m) 3.33.33.725.25.
Carrier gas He  HeHe
Substrate  Chromosorb G HP   
Column diameter (mm)    0.320.32
Phase thickness (mum)    1.1.
Temperature (C) 130.130.130.110.80.
I 872.0870.1874.869.866.
ReferenceDallos, Sisak, et al., 2000Reddy, Dutoit, et al., 1992Dutoit, 1991Samusenko and Golovnya, 1988Samusenko and Golovnya, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 20.25.35.35.35.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.230.250.250.250.25
Phase thickness (mum)  0.1560.1250.1250.125
Temperature (C) 150.80.80.80.80.
I 876.866.866.866.866.
ReferenceMorishita, Morimoto, et al., 1986Samusenko, Svetlova, et al., 1986Samusenko, Svetlova, et al., 1986Samusenko, Svetlova, et al., 1986Samusenko, Svetlova, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedPackedPacked
Active phase OV-101Apiezon LApolaneApiezon LPMS-100
Column length (m) 50.2.42.42.73.
Carrier gas HeHeHeN2 or HeHe
Substrate  Chromosorb W AW-DMCSChromosorbChromosorb G, AWCelite 545 (44-60 mesh)
Column diameter (mm) 0.25    
Phase thickness (mum) 0.125    
Temperature (C) 80.130.70.100.130.
I 868.903.863.8880.868.
ReferenceSamusenko, Svetlova, et al., 1986Shatts, Avots, et al., 1977Riedo, Fritz, et al., 1976Zhuravleva, Kapustin, et al., 1976Anderson, Jurel, et al., 1973
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPacked
Active phase PMS-100PMS-100
Column length (m) 3.3.
Carrier gas HeHe
Substrate Celite 545 (44-60 mesh)Celite 545 (44-60 mesh)
Column diameter (mm)   
Phase thickness (mum)   
Temperature (C) 150.180.
I 852.850.
ReferenceAnderson, Jurel, et al., 1973Anderson, Jurel, et al., 1973
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Dallos, Sisak, et al., 2000
Dallos, A.; Sisak, A.; Kulcsár, Z.; Kováts, E., Pair-wise interactions by gas chromatography VII. Interaction free enthalpies of solutes with secondary alcohol groups, J. Chromatogr. A, 2000, 904, 2, 211-242, https://doi.org/10.1016/S0021-9673(00)00908-0 . [all data]

Reddy, Dutoit, et al., 1992
Reddy, K.S.; Dutoit, J.-Cl.; Kovats, E. sz., Pair-wise interactions by gas chromatography. I. Interaction free enthalpies of solutes with non-associated primary alcohol groups, J. Chromatogr., 1992, 609, 1-2, 229-259, https://doi.org/10.1016/0021-9673(92)80167-S . [all data]

Dutoit, 1991
Dutoit, J., Gas chromatographic retention behaviour of some solutes on structurally similar polar and non-polar stationary phases, J. Chromatogr., 1991, 555, 1-2, 191-204, https://doi.org/10.1016/S0021-9673(01)87179-X . [all data]

Samusenko and Golovnya, 1988
Samusenko, A.L.; Golovnya, R.V., Prediction of the retention indices of methyl pyridines and pyrazines in capillary gas chromatography based on the non-linear additivity of the sorption energy, Chromatographia, 1988, 25, 6, 531-535, https://doi.org/10.1007/BF02324828 . [all data]

Morishita, Morimoto, et al., 1986
Morishita, F.; Morimoto, S.; Kojima, T., Prediction of molecular structures of aza-arenes by retention indices and fluorescence spectra, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 11, 688-692, https://doi.org/10.1002/jhrc.1240091120 . [all data]

Samusenko, Svetlova, et al., 1986
Samusenko, A.L.; Svetlova, N.I.; Golovnya, R.V., Reproducible and durable glass capillary columns with hydrogenated apiezon-l and OV-101 for the analysis of polar substances, Zh. Anal. Khim., 1986, 61, 1, 127-133. [all data]

Shatts, Avots, et al., 1977
Shatts, V.D.; Avots, A.A.; Belikov, V.A., Retention indices of alkylpyridines, Zh. Anal. Khim., 1977, 32, 4, 631-638. [all data]

Riedo, Fritz, et al., 1976
Riedo, F.; Fritz, D.; Tarján, G.; Kováts, E.Sz., A tailor-made C87 hydrocarbon as a possible non-polar standard stationary phase for gas chromatography, J. Chromatogr., 1976, 126, 63-83, https://doi.org/10.1016/S0021-9673(01)84063-2 . [all data]

Zhuravleva, Kapustin, et al., 1976
Zhuravleva, I.L.; Kapustin, Yu.P.; Golovnya, P.B., Retention indices of some isoaliphatic and heterocyclic nitrogenous bases, Zh. Anal. Khim., 1976, 31, 1378-1380. [all data]

Anderson, Jurel, et al., 1973
Anderson, A.; Jurel, S.; Shymanska, M.; Golender, L., Gas-liquid chromatography of some aliphatic and heterocyclic mono- and pollyfunctional amines. VII. Retention indices of amines in some polar and unpolar stationary phases, Latv. PSR Zinat. Akad. Vestis Kim. Ser., 1973, 1, 51-63. [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References