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Benzene, 1,3-dimethyl-

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Kovats' RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-20Supelcowax-10DB-WaxDB-WaxDB-Wax
Column length (m) 25.60.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 50.35.40.40.40.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 5.5.5.5.5.
Final hold (min)  20.   
I 1143.1142.1141.1143.1142.
ReferenceShimadzu, 2003Wong and Tie, 1993Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase DB-WaxCarbowax 20M
Column length (m) 60.50.
Carrier gas He 
Substrate   
Column diameter (mm) 0.250.22
Phase thickness (mum) 0.25 
Tstart (C) 40.80.
Tend (C) 200.200.
Heat rate (K/min) 3.2.
Initial hold (min) 5. 
Final hold (min)   
I 1143.1149.
ReferenceTatsuka, Suekane, et al., 1990Nishimura, Yamaguchi, et al., 1989
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Shimadzu, 2003
Shimadzu, Gas chromatography analysis of organic solvents using capillary columns (No. 2), 2003, retrieved from http://www.shimadzu.com/apps/form.cfm. [all data]

Wong and Tie, 1993
Wong, K.C.; Tie, D.Y., The Essential Oil of the Leaves of Murraya koenigii Spreng., J. Essent. Oil Res., 1993, 5, 4, 371-374, https://doi.org/10.1080/10412905.1993.9698245 . [all data]

Tatsuka, Suekane, et al., 1990
Tatsuka, K.; Suekane, S.; Sakai, Y.; Sumitani, H., Volatile constituents of kiwi fruit flowers: simultaneous distillation and extraction versus headspace sampling, J. Agric. Food Chem., 1990, 38, 12, 2176-2180, https://doi.org/10.1021/jf00102a015 . [all data]

Nishimura, Yamaguchi, et al., 1989
Nishimura, O.; Yamaguchi, K.; Mihara, S.; Shibamoto, T., Volatile Constituents of Guava Fruits (Psidium guajava L.) and Canned Puree, J. Agric. Food Chem., 1989, 37, 1, 139-142, https://doi.org/10.1021/jf00085a033 . [all data]


Notes

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