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Benzene, 1,3-dimethyl-

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Normal alkane RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeDB-1OV-101OV-101OV-101
Column length (m)  60.50.50.50.
Carrier gas  HeNitrogenNitrogenNitrogen
Substrate      
Column diameter (mm)  0.320.300.300.30
Phase thickness (mum)  1.0.260.260.26
Temperature (C) 120.60.100.100.100.
I 877.855.866.866.866.
ReferenceChen and Feng, 2006Shimadzu, 2003Gerasimenko and Nabivach, 1995Gerasimenko and Nabivach, 1995Gerasimenko and Nabivach, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SqualaneSqualaneOV-101OV-101
Column length (m) 50.  50.50.
Carrier gas Nitrogen    
Substrate      
Column diameter (mm) 0.30  0.200.20
Phase thickness (mum) 0.26    
Temperature (C) 100.100.100.100.100.
I 867.865.868.866.867.
ReferenceGerasimenko and Nabivach, 1995Berezkin, 1993Berezkin, 1993Tian, 1993Tian, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101Methyl SiliconeSqualaneSqualane
Column length (m) 50.50.74.6180.180.
Carrier gas   N2  
Substrate      
Column diameter (mm) 0.200.200.280.250.25
Phase thickness (mum)      
Temperature (C) 120.120.50.100.40.
I 870.871.849.862.847.
ReferenceTian, 1993Tian, 1993N/AKrupcik, Cellar, et al., 1986Krupcik, Cellar, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneOV-101OV-101E-301Squalane
Column length (m) 180.  50.50.
Carrier gas    N2N2
Substrate      
Column diameter (mm) 0.25  0.250.25
Phase thickness (mum)      
Temperature (C) 70.50.70.100.100.
I 855.853.858.871.867.
ReferenceKrupcik, Cellar, et al., 1986Wu and Lu, 1984Wu and Lu, 1984Bermejo, Moinelo, et al., 1980Bermejo, Moinelo, et al., 1980
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedPacked
Active phase SqualaneSqualaneDC-400Polydimethyl siloxane
Column length (m)  100.3.0 
Carrier gas H2N2Helium 
Substrate   Gas-Pak (60-80 mesh) 
Column diameter (mm)  0.25  
Phase thickness (mum)     
Temperature (C) 95.4110.150.110.
I 852.868.874.870.
ReferenceSojak and Vigdergauz, 1978Papazova and Pankova, 1975Anderson, 1968Ferrand, 1962
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Chen and Feng, 2006
Chen, Y.; Feng, C.-I., Regerating the spent metal-contaminated cracking catalyst by ozalic acid, J. Shanxi Univ. (Nat. Sci. Ed.), 2006, 29, 4, 414-420. [all data]

Shimadzu, 2003
Shimadzu, Gas chromatography analysis of organic solvents using capillary columns (No. 3), 2003, retrieved from http://www.shimadzu.com/apps/form.cfm. [all data]

Gerasimenko and Nabivach, 1995
Gerasimenko, V.A.; Nabivach, N.M., Principles of chromatographic retention of alkylbenzenes of stationary phases of different polarity, Koks i Khimia (in Russian) (Coke and Chemistry), 1995, 10, 20-27. [all data]

Berezkin, 1993
Berezkin, V.G., Linear correlation between retention indexes obtained in different laboratories on open tubular capillary columns with the same liquid stationary phase, Chem. Anal. (Warsaw), 1993, 38, 5, 649-651. [all data]

Tian, 1993
Tian, S., Analysis of the tower bottom oil of dimethylbenzene rectifying tower and C9 aromatic hydrocarbon fraction by capillary gas chromatography, Chin. J. Chromatogr., 1993, 11, 4, 202-206. [all data]

Krupcik, Cellar, et al., 1986
Krupcik, J.; Cellar, P.; Repka, D., Analyza cyklickych a aromatickych uhlovodnikov s poctom uhlikovych atomov 8 kapilarnou plynovou chromatografiou, Ropa a Uhlie, 1986, 28, 8, 485-495. [all data]

Wu and Lu, 1984
Wu, J.; Lu, W., Kovats indices of C4-C10 hydrocarbons in apolar quartz capillary OV-101, Chin. J. Chromatogr., 1984, 1, 1, 11-17. [all data]

Bermejo, Moinelo, et al., 1980
Bermejo, J.; Moinelo, S.R.; Suarez Canga, C., Calculo de indices de retencion a patir de DI y de la polaridad de la fase, Calculo de indices de retencion a patir de DI y de la polaridad de la fase, Instituto Nacional del Carbon y sus Derivados Francisco Pintado Fe (INCAR), La Corredoria, Oviedo, Espana, 1980, 13. [all data]

Sojak and Vigdergauz, 1978
Sojak, L.; Vigdergauz, M.S., Comparison of interpolation methods for the interpretation of retention data in gas chromatography, J. Chromatogr., 1978, 148, 1, 159-167, https://doi.org/10.1016/S0021-9673(00)99332-4 . [all data]

Papazova and Pankova, 1975
Papazova, D.I.; Pankova, M.C., Identification of individual aromatic hydrocarbons in kerosene fraction (b.p. 150-250 °), J. Chromatogr., 1975, 105, 2, 411-414, https://doi.org/10.1016/S0021-9673(01)82276-7 . [all data]

Anderson, 1968
Anderson, D.G., USe of Kovats retention indices and response factors for the qualitative and quantitative analysis of coating solvents, J. Paint Technol., 1968, 40, 527, 549-557. [all data]

Ferrand, 1962
Ferrand, R., Gas phase chromatography using retention indices for the analysis of tars and their hydrogenation products, Journees internationales d'etude des methodes de separation immediate at de chromatographie; Org. sur l'initiative du IX., 1962, 132-140. [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, isothermal, References