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1-Pentene, 2,4,4-trimethyl-

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Petrocol DHSqualaneOV-3OV-3OV-3
Column length (m) 150.93.   
Carrier gas H2He   
Substrate      
Column diameter (mm) 0.250.25   
Phase thickness (mum) 1.    
Temperature (C) 30.30.30.40.50.
I 708.6701.5712.0713.0714.0
ReferenceSoják, Addová, et al., 2004Soják, Addová, et al., 2004Chien, Furio, et al., 1983Chien, Furio, et al., 1983Chien, Furio, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-3OV-3OV-3OV-1OV-1
Column length (m)      
Carrier gas    H2H2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 60.70.80.30.40.
I 715.2716.4717.6709.9711.2
ReferenceChien, Furio, et al., 1983Chien, Furio, et al., 1983Chien, Furio, et al., 1983Chien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1OV-1SE-30
Column length (m)      
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 50.60.70.80.30.
I 712.5713.8715.3716.8710.2
ReferenceChien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m)      
Carrier gas H2H2H2H2H2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 40.50.60.70.80.
I 711.5711.9712.6717.1714.3
ReferenceChien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981Chien, Kopecni, et al., 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 1.  100.100.
Carrier gas He  N2N2
Substrate Chromaton N-AW-HMDS    
Column diameter (mm)    0.250.25
Phase thickness (mum)      
Temperature (C) 100.80.50.50.70.
I 715.708.704.704.707.
ReferenceNabivach and Kirilenko, 1980Chrétien and Dubois, 1977Chretien and Dubois, 1976Rijks and Cramers, 1974Rijks and Cramers, 1974
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPacked
Active phase SqualaneSqualaneSqualane
Column length (m) 91.410.10.
Carrier gas N2H2H2
Substrate    
Column diameter (mm) 0.25  
Phase thickness (mum)    
Temperature (C) 40.30.50.
I 706.702.704.
ReferenceMatukuma, 1969Tourres, 1967Tourres, 1967
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Soják, Addová, et al., 2004
Soják, L.; Addová, G.; Kubinec, R.; Kraus, A.; Bohác, A., Capillary gas chromatography-mass spectrometry of all 93 acyclic octenes and their identification in fluid catalytic cracked gasoline, J. Chromatogr. A, 2004, 1025, 2, 237-253, https://doi.org/10.1016/j.chroma.2003.10.112 . [all data]

Chien, Furio, et al., 1983
Chien, C.-F.; Furio, D.L.; Kopecni, M.M.; Laub, R.J., Specific retention volumes and retention indices of selected hydrocarbon solutes with OV-3, OV-7, OV-11, OV-17, OV-22, and OV-25 polymethylphenylsiloxane solvents, J. Hi. Res. Chromatogr., 1983, 6, 12, 669-679, https://doi.org/10.1002/jhrc.1240061207 . [all data]

Chien, Kopecni, et al., 1981
Chien, C.-F.; Kopecni, M.M.; Laub, R.J., Specific Retention Volumes and Retention Indices of Selected Hydrocarbon Solutes with OV-1 and SE-30 Polydimethylsiloxane Solvents, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1981, 4, 10, 539-543, https://doi.org/10.1002/jhrc.1240041017 . [all data]

Nabivach and Kirilenko, 1980
Nabivach, V.M.; Kirilenko, A.V., Relationship between the gas chromatographic behaviour and the molecular structure of hydrocarbon samples and various stationary phases. Part II. Correlation between the retention index, physicochemical properties and molecular structure, Chromatographia, 1980, 13, 2, 93-100, https://doi.org/10.1007/BF02263060 . [all data]

Chrétien and Dubois, 1977
Chrétien, J.R.; Dubois, J.E., Topological analysis of gas-liquid chromatographic behavior of alkenes, Anal. Chem., 1977, 49, 6, 747-756, https://doi.org/10.1021/ac50014a021 . [all data]

Chretien and Dubois, 1976
Chretien, J.R.; Dubois, J.-E., New Perspectives in the Prediction of Kovats Indices, J. Chromatogr., 1976, 126, 171-189, https://doi.org/10.1016/S0021-9673(01)84071-1 . [all data]

Rijks and Cramers, 1974
Rijks, J.A.; Cramers, C.A., High precision capillary gas chromatography of hydrocarbons, Chromatographia, 1974, 7, 3, 99-106, https://doi.org/10.1007/BF02269819 . [all data]

Matukuma, 1969
Matukuma, A., Retention indices of alkanes through C10 and alkenes through C8 and relation between boiling points and retention data, Gas Chromatogr., Int. Symp. Anal. Instrum. Div Instrum Soc. Amer., 1969, 7, 55-75. [all data]

Tourres, 1967
Tourres, D.A., Structural analysis of industrial butene dimers by gas chromatography, J. Gas Chromatogr., 1967, 5, 1, 35-40, https://doi.org/10.1093/chromsci/5.1.35 . [all data]


Notes

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