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Propyl mercaptan

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase DB-5DB-5DB-5DB-5Apiezon M
Column length (m) 30.30.30.30.2.1
Carrier gas     He or N2
Substrate     Chromosorb W, AW-DMCS
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.10.10.10.1 
Temperature (C) 100.120.60.80.130.
I 617.0630.0615.4615.7623.
ReferenceMiller and Bruno, 2003Miller and Bruno, 2003Miller and Bruno, 2003Miller and Bruno, 2003Garbuzov, Misharina, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SqualaneSqualaneApiezon MDC-200SE-30
Column length (m) 2.2.2.11.51.5
Carrier gas   N2  
Substrate Chromosorb W DMCSChromosorb W DMCSChromosorb W  
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 60.80.130.60.60.
I 586.590.619.603.600.
ReferenceZygmunt and Staszewski, 1981Zygmunt and Staszewski, 1981Golovnya and Garbuzov, 1974Golovnya and Arsen'ev, 1970Golovnya and Arsen'ev, 1970
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Miller and Bruno, 2003
Miller, K.E.; Bruno, T.J., Isothermal Kováts retention indices of sulfur compounds on a poly(5% diphenyl-95% dimethylsiloxane) stationary phase, J. Chromatogr. A, 2003, 1007, 1-2, 117-125, https://doi.org/10.1016/S0021-9673(03)00958-0 . [all data]

Garbuzov, Misharina, et al., 1985
Garbuzov, V.G.; Misharina, T.A.; Aerov, A.F.; Golovnya, R.V., Gas chromatographic retention indices for sulphur(II)-containing organic substances, J. Anal. Chem. USSR (Engl. Transl.), 1985, 40, 4, 576-586. [all data]

Zygmunt and Staszewski, 1981
Zygmunt, B.; Staszewski, R., Retention index and gas chromatographic-mass spectrometric identification of thiols in liquified gas, Chem. Anal. (Warsaw), 1981, 26, 109-113. [all data]

Golovnya and Garbuzov, 1974
Golovnya, R.V.; Garbuzov, V.G., Effect of heteroatom in aliphatic sulfur- and oxygen-containing compounds on the values of the retention indices in gas chromatography, Izv. Akad. Nauk SSSR Ser. Khim., 1974, 7, 1519-1521. [all data]

Golovnya and Arsen'ev, 1970
Golovnya, R.V.; Arsen'ev, Y.N., Gas-chromatographic method for the analysis of n-mercaptans and symmetrical n-sulfides and n-disulfides, Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.), 1970, 6, 4, 1316-1318, https://doi.org/10.1007/BF00852683 . [all data]


Notes

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