p-Xylene

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Normal alkane RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeDB-1SqualaneSqualaneOV-101
Column length (m)  60.  50.
Carrier gas  He   
Substrate      
Column diameter (mm)  0.32  0.20
Phase thickness (μm)  1.   
Temperature (C) 120.60.100.100.100.
I 872.856.861.868.866.
ReferenceChen and Feng, 2006Shimadzu, 2003Berezkin, 1993Berezkin, 1993Tian, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101Methyl SiliconeSqualane
Column length (m) 50.50.50.74.6180.
Carrier gas    N2 
Substrate      
Column diameter (mm) 0.200.200.200.280.25
Phase thickness (μm)      
Temperature (C) 100.120.120.50.100.
I 868.870.872.852.860.
ReferenceTian, 1993Tian, 1993Tian, 1993N/AKrupcik, Cellar, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneOV-101OV-101E-301
Column length (m) 180.180.  50.
Carrier gas     N2
Substrate      
Column diameter (mm) 0.250.25  0.25
Phase thickness (μm)      
Temperature (C) 40.70.50.70.100.
I 845.853.854.857.870.
ReferenceKrupcik, Cellar, et al., 1986Krupcik, Cellar, et al., 1986Wu and Lu, 1984Wu and Lu, 1984Bermejo, Moinelo, et al., 1980
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedPacked
Active phase SqualaneSqualaneSqualaneApiezon LDC-400
Column length (m) 50. 100.3.23.0
Carrier gas N2H2N2 Helium
Substrate     Gas-Pak (60-80 mesh)
Column diameter (mm) 0.25 0.25  
Phase thickness (μm)      
Temperature (C) 100.95.4110.100.150.
I 864.850.865.890.874.
ReferenceBermejo, Moinelo, et al., 1980Sojak and Vigdergauz, 1978Papazova and Pankova, 1975Kavan, 1973Anderson, 1968
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase Polydimethyl siloxane
Column length (m)  
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (μm)  
Temperature (C) 110.
I 870.
ReferenceFerrand, 1962
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Chen and Feng, 2006
Chen, Y.; Feng, C.-I., Regerating the spent metal-contaminated cracking catalyst by ozalic acid, J. Shanxi Univ. (Nat. Sci. Ed.), 2006, 29, 4, 414-420. [all data]

Shimadzu, 2003
Shimadzu, Gas chromatography analysis of organic solvents using capillary columns (No. 3), 2003, retrieved from http://www.shimadzu.com/apps/form.cfm. [all data]

Berezkin, 1993
Berezkin, V.G., Linear correlation between retention indexes obtained in different laboratories on open tubular capillary columns with the same liquid stationary phase, Chem. Anal. (Warsaw), 1993, 38, 5, 649-651. [all data]

Tian, 1993
Tian, S., Analysis of the tower bottom oil of dimethylbenzene rectifying tower and C9 aromatic hydrocarbon fraction by capillary gas chromatography, Chin. J. Chromatogr., 1993, 11, 4, 202-206. [all data]

Krupcik, Cellar, et al., 1986
Krupcik, J.; Cellar, P.; Repka, D., Analyza cyklickych a aromatickych uhlovodnikov s poctom uhlikovych atomov 8 kapilarnou plynovou chromatografiou, Ropa a Uhlie, 1986, 28, 8, 485-495. [all data]

Wu and Lu, 1984
Wu, J.; Lu, W., Kovats indices of C4-C10 hydrocarbons in apolar quartz capillary OV-101, Chin. J. Chromatogr., 1984, 1, 1, 11-17. [all data]

Bermejo, Moinelo, et al., 1980
Bermejo, J.; Moinelo, S.R.; Suarez Canga, C., Calculo de indices de retencion a patir de DI y de la polaridad de la fase, Calculo de indices de retencion a patir de DI y de la polaridad de la fase, Instituto Nacional del Carbon y sus Derivados Francisco Pintado Fe (INCAR), La Corredoria, Oviedo, Espana, 1980, 13. [all data]

Sojak and Vigdergauz, 1978
Sojak, L.; Vigdergauz, M.S., Comparison of interpolation methods for the interpretation of retention data in gas chromatography, J. Chromatogr., 1978, 148, 1, 159-167, https://doi.org/10.1016/S0021-9673(00)99332-4 . [all data]

Papazova and Pankova, 1975
Papazova, D.I.; Pankova, M.C., Identification of individual aromatic hydrocarbons in kerosene fraction (b.p. 150-250 °), J. Chromatogr., 1975, 105, 2, 411-414, https://doi.org/10.1016/S0021-9673(01)82276-7 . [all data]

Kavan, 1973
Kavan, I., Analysis of odorants, Sbornik Praci UVP, 1973, 26, 128-144. [all data]

Anderson, 1968
Anderson, D.G., USe of Kovats retention indices and response factors for the qualitative and quantitative analysis of coating solvents, J. Paint Technol., 1968, 40, 527, 549-557. [all data]

Ferrand, 1962
Ferrand, R., Gas phase chromatography using retention indices for the analysis of tars and their hydrogenation products, Journees internationales d'etude des methodes de separation immediate at de chromatographie; Org. sur l'initiative du IX., 1962, 132-140. [all data]


Notes

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