2,6-Octadienal, 3,7-dimethyl-, (Z)-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Equity-5MSHP-5DB-5SLB-5MSSLB-5MS
Column length (m) 30.30.30.10.10.
Carrier gas HeN2He  
Substrate      
Column diameter (mm) 0.250.250.320.10.1
Phase thickness (μm) 0.250.250.50.10.1
Tstart (C) 50.50.40.40.40.
Tend (C) 250.220.265.250.250.
Heat rate (K/min) 3.5.7.40.40.
Initial hold (min)  10.   
Final hold (min) 10. 5.  
I 1239.1243.1242.1231.1244.
ReferenceBelsito E.L., Carbone C., et al., 2007Flamini, Tebano, et al., 2007Mahattanatawee K., Perez-Cacho P.R., et al., 2007Mondello, Sciarrone, et al., 2007Mondello, Sciarrone, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5MSSLB-5MSRTX-1Equity-5DB-5
Column length (m) 10.10.60.60.30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.10.10.220.250.22
Phase thickness (μm) 0.10.10.251.0.25
Tstart (C) 40.40.60.40.55.
Tend (C) 250.250.230.260.240.
Heat rate (K/min) 40.40.2.5.3.
Initial hold (min)    1.2.
Final hold (min)   35.15.15.
I 1245.1245.1214.1211.1240.
ReferenceMondello, Sciarrone, et al., 2007Mondello, Sciarrone, et al., 2007Paolini J., Costa J., et al., 2007Rocha, Coelho, et al., 2007Silva, Barbosa, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSPB-1SPB-1DB-1SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.2
Phase thickness (μm) 0.250.20.250.250.2
Tstart (C) 60.70.50.50.70.
Tend (C) 280.220.250.265.220.
Heat rate (K/min) 3.3.5.2.53.
Initial hold (min)   3.  
Final hold (min)  15.15. 15.
I 1235.1214.1218.1216.1214.
ReferenceKukic J., Petrovic S., et al., 2006Pinto, Pina-Vaz, et al., 2006Radulovic, Mananjarasoa, et al., 2006Ramezani, Behravan, et al., 2006Salgueiro L.R., Pinto E., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-1DB-5DB-1MDN-5
Column length (m) 30.50.60.30.30.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.250.220.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.70.50.50.
Tend (C) 280.220.230.250.250.
Heat rate (K/min) 4.2.2.2.3.
Initial hold (min) 5. 2.8. 
Final hold (min)  20.20.  
I 1237.1213.1235.1221.1235.
ReferenceSaroglou, Dorizas, et al., 2006Boti J.B., Koukoua G., et al., 2005Choi, 2005Dob, Dahmane, et al., 2005Dugo, Mondello, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1ZB-5HP-5MSHP-5MS
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.2
Phase thickness (μm) 0.250.250.50.250.25
Tstart (C) 40.40.40.60.60.
Tend (C) 250.250.265.250.200.
Heat rate (K/min) 3.3.7.4.2.
Initial hold (min)    2. 
Final hold (min) 20.20.5.20.10.
I 1213.1214.1236.1240.1242.
ReferenceFanciullino, Gancel, et al., 2005Gancel, Ollitrault, et al., 2005Mahattanatawee, Rouseff, et al., 2005Pino, Mesa, et al., 2005Smadja, Rondeau, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Mega 5MSHP-5MSRTX-5HP-5DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 40.60.45.60.40.
Tend (C) 240.280.300.260.280.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min) 2. 6. 2.
Final hold (min)   10.  
I 1231.1236.1242.1240.1241.
ReferenceVerzera, Trozzi, et al., 2005Chorianopoulos, Kalpoutzakis, et al., 2004Dugo, Mondello, et al., 2004Javidnia, Miri, et al., 2004Mardarowicz, Wianowska, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200HP-5SPB-1SPB-1SPB-1
Column length (m) 30.25.30.30.25.
Carrier gas H2HeHeHe 
Substrate      
Column diameter (mm) 0.320.20.20.250.25
Phase thickness (μm) 0.250.330.20.250.25
Tstart (C) 40.60.70.35.35.
Tend (C) 280.240.220.225.225.
Heat rate (K/min) 6.3.3.4.4.
Initial hold (min) 5.  5.10.
Final hold (min) 5.7.15.20. 
I 1244.1238.1214.1212.1215.
ReferenceNgassoum, Ousmaila, et al., 2004Sartoratto, Machado, et al., 2004Cavaleiro, Salgueiro, et al., 2003Chisholm, Jell, et al., 2003Chisholm, Wilson, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1DB-5DB-1DB-5
Column length (m) 25.25.30.30.30.
Carrier gas   N2He 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 35.35.70.40.40.
Tend (C) 225.225.230.250.265.
Heat rate (K/min) 4.4.2.3.7.
Initial hold (min) 10.10.2.  
Final hold (min)   20.20.5.
I 1215.1215.1235.1214.1273.
ReferenceChisholm, Wilson, et al., 2003Chisholm, Wilson, et al., 2003Choi, 2003Gancel, Ollitrault, et al., 2003Högnadóttir and Rouseff, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSHP-5MS5
Column length (m) 30.30.60.30.25.
Carrier gas HeN2HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 75.75.40.60.40.
Tend (C) 230.230.310.280.180.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min) 10.10.1.  
Final hold (min) 20. 20.  
I 1241.1247.1245.1240.1240.
ReferenceJantan, Ling, et al., 2003bin Jantan, Yassin, et al., 2003Lalel, Singh, et al., 2003Ngassapa, Runyoro, et al., 2003Shao, Marriott, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5Mega 5MSSPB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm) 0.250.250.250.200.25
Tstart (C) 40.60.40.70.50.
Tend (C) 240.240.240.220.280.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)   2. 5.
Final hold (min)    15. 
I 1244.1242.1231.1240.1240.
ReferenceShellie and Marriott, 2003Tampieri, Galuppi, et al., 2003Verzera, Trozzi, et al., 2003Cavaleiro, Salgueiro, et al., 2002Demetzos, Angelopoulou, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1RTX-5HP-1CP Sil 5 CBDB-1
Column length (m) 50.30.24.30.50.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.220.250.320.250.22
Phase thickness (μm) 0.250.250.170.250.25
Tstart (C) 60.45.60.60.60.
Tend (C) 220.300.250.280.220.
Heat rate (K/min) 2.3.4.2.2.
Initial hold (min)  6.2.10. 
Final hold (min) 20.10.20.40.20.
I 1213.1241.1212.1239.1214.
ReferenceLota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002Nath, Sarma, et al., 2002Pino, Marbot, et al., 2002Pintore, Usai, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1SE-30DB-1BP-1
Column length (m) 15.15.25.30.50.
Carrier gas   N2 He
Substrate      
Column diameter (mm) 0.250.250.200.320.22
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 35.35.60.40.60.
Tend (C) 225.225.180.240.220.
Heat rate (K/min) 6.6.3.7.2.
Initial hold (min) 3.3.10.  
Final hold (min) 10.10.1.5. 
I 1215.1215.1247.1228.1213.
ReferenceChisholm, Wilson, et al., 2001Chisholm, Wilson, et al., 2001bin Jantan, Basni, et al., 2001Lin and Rouseff, 2001Lota, Serra, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 5 CBHP-5MSHP-5DB-5
Column length (m) 50.50.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.320.250.200.25
Phase thickness (μm) 0.250.40.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 220.280.280.180.290.
Heat rate (K/min) 2.3.4.4.4.
Initial hold (min)  10.5.8.2.
Final hold (min)  60. 2.5.
I 1213.1215.1240.1240.1225.
ReferenceLota, Serra, et al., 2001Pino and Marbot, 2001Skaltsa, Mavrommati, et al., 2001Alonzo, Bosco, et al., 2000Bartley and Jacobs, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1RTX-5Mega 5MSMega 5MSCBP-1
Column length (m) 50.10.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.10.250.250.25
Phase thickness (μm) 0.250.10.250.25 
Tstart (C) 60.50.40.40.60.
Tend (C) 230.350.240.240.240.
Heat rate (K/min) 2.12.33.3.4.
Initial hold (min)   2.2. 
Final hold (min) 35.    
I 1213.1248.1231.1231.1218.
ReferenceLota, de Rocca Serra, et al., 2000Mondello, Zappia, et al., 2000Verzera, la Rosa, et al., 2000Verzera, Trozzi, et al., 2000Zunino, Lopez, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1Methyl SiliconeDB-5DB-1
Column length (m) 50.50.50.30.60.
Carrier gas HeHeN2  
Substrate      
Column diameter (mm) 0.220.220.250.250.32
Phase thickness (μm) 0.250.250.170.250.5
Tstart (C) 60.60.80.50.40.
Tend (C) 230.230.200.250.290.
Heat rate (K/min) 2.2.2.3.4.
Initial hold (min)     2.
Final hold (min) 35.35.  5.
I 1213.1213.1228.1241.1220.
ReferenceLota, Serra, et al., 1999Lota, Serra, et al., 1999Sumathykutty, Rao, et al., 1999Isidorov, Zenkevich, et al., 1998Bartley and Foley, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-101OV-101OV-101OV-101
Column length (m) 60.50.50.50.50.
Carrier gas HeN2N2N2H2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.25    
Tstart (C) 70.70.80.80.50.
Tend (C) 250.200.200.200.200.
Heat rate (K/min) 2.53.2.2.2.
Initial hold (min) 5.    
Final hold (min) 15.    
I 1208.1231.1218.1219.1213.
ReferenceCombariza, Tirado, et al., 1994Chung, Eiserich, et al., 1993Yang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Pieribattesti, Smadja, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References