2,6-Octadien-1-ol, 3,7-dimethyl-, (E)-

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Normal alkane RI, polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelco CO Wax-10InnowaxDB-WaxHP InnowaxInnowax FSC
Column length (m) 60.60.30.60.60.
Carrier gas Helium Helium Helium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.330.250.330.25
Program 35 0C (6 min) 2 0C/min -> 60 0C (5 min) 5 0C/min -> 200 0C 25 0C/min -> 250 0C (6 min)not specifiednot specifiednot specified60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C
I 1852.1857.1895.1857.1857.
ReferencePrompona, Kandylis, et al., 2012Noorizadeh, Farmany, et al., 2011Zeng, Xie, et al., 2011Noorizadeh and Farmany, 2010Polatoglu, Demirci, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCCP-Wax 52 CBDB-WaxDB-WaxHP Innowax
Column length (m) 60.50.15.15.50.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (μm) 0.250.200.250.250.25
Program 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C60 0C (5 min) 3 0C/min -> 250 0C (20 min) 1 0C/min -> 255 0C50 0C (5 min) 6 0C/min -> 125 0C 10 0C/min -> 170 0C50 0C (5 min) 6 0C/min -> 125 0C 10 0C/min -> 170 0C40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
I 1857.1847.1829.1832.1857.
ReferenceBaser, Demirci, et al., 2009Genisheva and Oliveira, 2009Keefover-Ring, Thompson, et al., 2009Keefover-Ring, Thompson, et al., 2009Mancini, Arnold, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCP-Wax 52 CBSupelcowax 10DB-WaxHP-Innowax FSC
Column length (m) 30.50.50.30.60.
Carrier gas HeliumHeliumHeliumHeliumN2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.290.250.250.25
Program not specified33 0C (1 min) 2 0C/min -> 130 0C 10 0C/min -> 220 0C45 0C (15 min) 3 0C/min -> 75 0C 5 0C/min -> 180 0C (10 min)40 0C (4 min) 3 0C/min -> 50 0C 5 0C/min -> 120 0C 7 0C/min -> 175 0C 10 0C/min -> 230 0C (8 min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1845.1802.1852.1856.1857.
ReferenceZhao, Xu, et al., 2009Kaack and Christensen, 2008Soria, Martinez-Castro, et al., 2008Yongsheng, Hua, et al., 2008Baser K.H.C. and Demirci B., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPHP-InnowaxHP Innowax FSPDB-WaxInnowax FSC
Column length (m) 30.30.60.30.60.
Carrier gas HeHeliumN2 N2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40C(1min) => 7C/min => 180C => 10C/min => 240C (10min)30 0C (5 min) 5 0C/min -> 100 0C (5 min) 1 0C/min -> 130 0C 10 0C/min -> 195 0C (45 min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C40 0C (3 min) 3 0C/min -> 150 0C (2 min) 6 0C/min -> 230 0C (10 min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1835.1797.1857.1849.1857.
ReferenceGreger and Schieberle, 2007Narain, Galvao, et al., 2007Tabanca N., Demirci B., et al., 2007Wenguang, Wenlai, et al., 2007Iscan, Kirimer, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxHP-Innowax FSCDB-WaxHP-InnowaxInnowax FSC
Column length (m) 50.60.30.60.60.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.250.250.25
Program 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C60(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1857.1857.1797.1857.1857.
ReferenceSenatore, Apostolides Arnold, et al., 2006Suleimenov Y.M., Atazhanova G.A., et al., 2006Berlinet, Ducruet, et al., 2005Duman, Kartal, et al., 2005Kosar, Özek, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCDB-FFAPHP-Innowax FSCHP-Innowax FSCBP-21
Column length (m) 60.30.60.60.50.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.320.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C40C(2min) => 40C/min => 60C(2min) => 6C/min => 180C => 15C/min => 230C (10min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C50C => 2.5C/min => 180C(2min) => 1C/min => 200C(10min)
I 1857.1818.1857.1857.1860.
ReferenceBaser, Özek, et al., 2004Buettner, 2004Demirci, Paper, et al., 2004Demirci, Paper, et al., 2004, 2Salinas, Zalacain, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MCarbowax 20MHP-Innowax FSCInnowax FSCHP-Innowax FSC
Column length (m)   60.60.60.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm)   0.250.250.25
Phase thickness (μm)   0.250.250.25
Program not specifiednot specified60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1843.1843.1857.1857.1857.
ReferenceVinogradov, 2004Vinogradov, 2004Demirci, Baser, et al., 2003Demirci and Baser, 2003Demirci, Dadandi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-Innowax FSCDB-WaxHP-InnowaxInnowax
Column length (m) 60.60.30.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.50.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C(40min)60C(2min) => 2C/min => 220C => 3C/min => 245C(20min)60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1857.1857.1840.1857.1857.
ReferenceErdemoglu, Sener, et al., 2003Kürkcüoglu, Demirci, et al., 2003Selli, Cabaroglu, et al., 2003Baser, Demirci, et al., 2002Baser, Nuriddinov, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCSupelcowax-10HP-InnowaxHP-InnowaxHP-Innowax FSC
Column length (m) 60.60.60.60.60.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C40C(20min) => (1.5C/min) => 200C => (10C/min) => 250C(120min)60 0C (10 min) 10 K/min -> 220 0C (10 min) 1K/min -> 240 0C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 1857.1835.1857.1857.1857.
ReferenceHüsnü Can Baser, Demirci, et al., 2002Rogerson and de Freitas, 2002Baser, Demirci, et al., 2001Gören, Demirci, et al., 2001Kaya, Demirci, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCDB-WaxHP-Innowax FSCFFAPInnowax
Column length (m) 60.30.60.50.60.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.50.250.33 
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C30C => 70C/min => 60C (3min) => 3C/min => 245C (20min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(1min) => 2.5C/min => 115C => 1C/min => 210C(30min)60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
I 1857.1832.1857.1828.1857.
ReferenceKivcak B., Mert T., et al., 2001Schneider, Razungles, et al., 2001Tabanca, Kirimer, et al., 2001Tucker, Maciarello, et al., 2001Ahmed, Choudhary, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCHP-Innowax FSCFFAPPEGPEG
Column length (m) 60.60.30.40.40.
Carrier gas HeHe HydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.320.1820.182
Phase thickness (μm) 0.250.250.250.300.30
Program 60C(10 min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C(20min)not specified35 0C (5 min) 5 0C/min -> 100 0C 3 0C/min -> 200 0C (1 min) 20 0C/min -> 240 0C (2 min)35 0C (5 min) 5 0C/min -> 100 0C 3 0C/min -> 200 0C (1 min) 20 0C/min -> 240 0C (2 min)
I 1856.1857.1845.1868.1873.
ReferenceKirimer, Tabanca, et al., 2000Kamariah, Lim, et al., 1999Lambert, Demazeau, et al., 1999Vas, Gal, et al., 1998Vas, Gal, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-FFAPCP-Wax 52CBSupelcowax 10Supelcowax 10
Column length (m) 60.30.25.60.60.
Carrier gas N2 H2HeliumHelium
Substrate      
Column diameter (mm)  0.320.30.250.25
Phase thickness (μm) 0.250.251.20.250.25
Program not specified35C (1min) => 40C/min => 60C (1min) => 6C/min => 250C (10min)60C(3min) => 2C/min => 220C => 3C/min => 245C60 0C (10 min) 2 0C/min -> 80 0C 3 0C/min -> 100 0C 4 0C/min -> 220 0C (30 min)not specified
I 1851.1840.1858.1832.1829.
ReferenceWeyerstahl, Marschall, et al., 1998Guth, 1997López-Tamames, Carro-Mariño, et al., 1997Castioni and Kapetanidis, 1996Castioni and Kapetanidis, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax 10CP-Wax 52 CBSupelcowaxSupelcowax-10NB-351
Column length (m) 60.30.30.30.25.
Carrier gas HeliumH2   
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (μm) 0.25   0.2
Program not specified60 0C 2 0C/min -> 220 0C 3 0C/min -> 245 0Cnot specifiednot specified40C(5min) => 4C/min => 150C => 8C/min => 240C(12min)
I 1840.1858.1849.1840.1862.
ReferenceCastioni and Kapetanidis, 1996Carro Marino, López Tamames, et al., 1995Garneau, Bouhajib, et al., 1994Jean, Garneau, et al., 1993Kerrola and Kallio, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCarbowax 20MCarbowax 20M
Column length (m) 30.60.  
Carrier gas   He 
Substrate     
Column diameter (mm) 0.250.32  
Phase thickness (μm) 0.25   
Program not specifiednot specifiednot specifiednot specified
I 1834.1849.1802.1797.
ReferenceMarlatt, Ho, et al., 1992Binder and Flath, 1989Peppard and Ramus, 1988Shibamoto, 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Prompona, Kandylis, et al., 2012
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Demirci, Dadandi, et al., 2003
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Erdemoglu, Sener, et al., 2003
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Notes

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