2,6-Octadien-1-ol, 3,7-dimethyl-, (E)-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-5 MSHP-5 MSHP-5 MSRTX-1
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 300.240.230.250.230.
Heat rate (K/min) 4.3.3.3.2.
Initial hold (min) 3.  1. 
Final hold (min) 15.  20.5.
I 1252.1263.1263.1264.1235.
ReferenceBertuzzi, Tirillini, et al., 2013Pinheiro, de Queiros, et al., 2013Pripdeevech and Saansoomchai, 2013Sardashti, Valizadeh, et al., 2013Bendiabdellah, El Amine Dib, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5HP-5SE-30 MSHP-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.100.60.50.40.
Tend (C) 230.260.240.250.260.
Heat rate (K/min) 2.10.3.5.4.
Initial hold (min)  1.2.5. 
Final hold (min) 5.10. 10.5.
I 1235.1266.1255.1255.1255.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Boukhris, Bouaziz, et al., 2012Kahriman, Tosun, et al., 2011Menichini, Tundis, et al., 2011Miyazawa, Marumoto, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5DB-5 MSOV-1HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.300.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 30.50.50.50.60.
Tend (C) 250.300.240.250.240.
Heat rate (K/min) 5.50.3.5.3.
Initial hold (min) 3.5. 3.2.
Final hold (min) 10.5. 2. 
I 1295.1251.1258.1238.1255.
ReferenceZarai, Kadri, et al., 2011Bi Kouame, Bedi, et al., 2010Chalchat, Figueredo, et al., 2010Hu, Liang, et al., 2010Kahriman, Tosun, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSBP-1HP-5 MSHP-5 MSHP-5 MS
Column length (m) 60. 30.30.30.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.25 0.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.60.100.70.70.
Tend (C) 250.220.220.290.290.
Heat rate (K/min) 5.5.2.5.5.
Initial hold (min) 15.10.   
Final hold (min) 15.30. 10.10.
I 1249.1238.1253.1256.1250.
ReferenceMesa-Arango, Betancur-Galvis, et al., 2010Mishra, Chaudhary, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1ZB-5SPB-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas NitrogenHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.530.25
Phase thickness (μm) 0.250.250.250.500.25
Tstart (C) 60.50.50.50.50.
Tend (C) 250.220.240.210.250.
Heat rate (K/min) 4.4.3.3.5.
Initial hold (min) 1.2. 5.2.
Final hold (min) 10.2.1.45. 
I 1235.1241.1225.1280.1253.
ReferenceSafaei-Ghomi, Meshkatalsadat, et al., 2010Xu, Tang, et al., 2010Gardini, Beletti, et al., 2009Gilani, Shah, et al., 2009Ho, Wang, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5 MSBP-1HP-5 MS
Column length (m) 50.30.30.50.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.200.250.250.220.25
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.50.50.60.70.
Tend (C) 220.250.250.220.290.
Heat rate (K/min) 5.5.2.2.5.
Initial hold (min) 3. 5.  
Final hold (min)    20.10.
I 1255.1253.1253.1240.1257.
ReferenceKazemi and Akhavani, 2009Koba, Catherine, et al., 2009Koba, Sanda, et al., 2009Ottavioli, Bighelli, et al., 2009Radulovic, Blagojevic, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1 MSHP-5MSDB-5BPX-5BPX-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.60.100.60.
Tend (C) 250.240.220.999.999.
Heat rate (K/min) 6.5.3.3.3.
Initial hold (min) 1.    
Final hold (min) 4.    
I 1236.1255.1253.1258.1259.
ReferenceSeo, Kim, et al., 2009Wannes, Mhamdi, et al., 2009Bastos, Ishimoto, et al., 2008Bieri and Marriott, 2008Bieri and Marriott, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5BPX-5BPX-5BPX-5ZB-1
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHydrogenHydrogenHydrogenNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.45.
Tend (C) 999.999.999.999.230.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min)      
Final hold (min)      
I 1259.1260.1262.1260.1234.
ReferenceBieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008Mierendorff, Stahl-Biskup, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Equity-5 MSHP-5HP-5 MSHP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumNitrogenHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.320.25
Tstart (C) 40.100.50.60.60.
Tend (C) 260.200.240.250.240.
Heat rate (K/min) 1.55.3.5.3.
Initial hold (min)  1. 30. 
Final hold (min)  15.   
I 1255.1255.1265.1254.1239.
ReferenceMondello, Casilli, et al., 2008Saeidnia and Hadjiakhoondi, 2008Sarikurkcu, Tepe, et al., 2008Yassa and Akhani, 2008Argyropoulou, Daferera, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5HP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.260.260.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 240.240.290.250.250.
Heat rate (K/min) 5.3.3.2.2.
Initial hold (min)    8.8.
Final hold (min)    15.15.
I 1236.1252.1252.1271.1250.
ReferenceAsekun, Olusegun, et al., 2007Bos, Woerdenbag, et al., 2007Elfami, Bos, et al., 2007Ferhat, Meklati, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1Col-Elite 5MSDBP-5BP-1HP-5 MS
Column length (m) 60.30.25. 30.
Carrier gas NitrogenHeHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (μm) 0.250.250.22 0.25
Tstart (C) 60.30.40.60.60.
Tend (C) 250.246.250.220.220.
Heat rate (K/min) 4.3.3.5.6.
Initial hold (min) 1. 1.  
Final hold (min) 10. 10.6. 
I 1237.1274.1218.1240.1232.
ReferenceGhasempour, Shirinpour, et al., 2007Gudaityte and Venskutonis R.P., 2007Heravi and Sereshti, 2007Kiran, Devi, et al., 2007Loghmani-Khouzani, Fini, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSSE-30HP-5DB-1DB-1
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeHeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.50.95.
Tend (C) 220.250.250.260.240.
Heat rate (K/min) 6.5.5.2.54.
Initial hold (min)  5.5.1. 
Final hold (min)  10.10.20. 
I 1255.1255.1235.1233.1250.
ReferenceLoghmani-Khouzani, Fini, et al., 2007Loizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Monser-Esfahani, Karamkhani, et al., 2007Pala-Paul, Brophy, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1HP-5 MSDBP-5DB-5
Column length (m) 25.60.60.25.30.
Carrier gas HeliumNitrogenHydrogenHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.220.25
Tstart (C) 100.60.60.40.60.
Tend (C) 280.250.260.250.320.
Heat rate (K/min) 4.4.4.3.10.
Initial hold (min) 3.1. 1. 
Final hold (min) 5.10.20.10.4.
I 1258.1237.1259.1218.1256.
ReferencePhutdhawong, Kawaree, et al., 2007Reza, Ebrahim, et al., 2007Rojas, Velasco, et al., 2007Sereshti and Samadi, 2007Smelcerovic, Spiteller, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Elite-5MSDB-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas  HeHeliumHelium 
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.5  0.25
Tstart (C) 40.40.60.60.40.
Tend (C) 250.280.200.200.240.
Heat rate (K/min) 2.4.2.2.5.
Initial hold (min)  5.  3.
Final hold (min) 33.10.20.20.10.
I 1260.1251.1250.1255.1239.
ReferenceSylvestre, Pichette, et al., 2007Tava, Pecetti, et al., 2007Tiwary, Nail, et al., 2007Tiwary, Nail, et al., 2007Wenguang, Wenlai, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5BP-1BP-1DB-5
Column length (m) 30.60.50.50.30.
Carrier gas HeHeHe Helium
Substrate      
Column diameter (mm) 0.250.250.220.220.26
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 250.250.220.220.290.
Heat rate (K/min) 5.3.2.2.3.
Initial hold (min) 30.    
Final hold (min)   20.20. 
I 1254.1252.1229.1233.1252.
ReferenceYassa and Akhani, 2007Bertrand, Comte, et al., 2006Boti, Muselli, et al., 2006Boti, Yao, et al., 2006Elfami, Komar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5MSHP-5CP Sil 5 CBFSOT-RSL-200
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHe Hydrogen
Substrate      
Column diameter (mm) 0.220.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.40.40.
Tend (C) 220.250.300.220.280.
Heat rate (K/min) 2.2.5.3.6.
Initial hold (min)   5. 5.
Final hold (min) 20. 5.3.5.
I 1232.1255.1265.1253.1253.
ReferenceFanciullino, Tomi, et al., 2006Farah, Afifi, et al., 2006Figuérédo, Cabassu, et al., 2006Hymete, Rohloff, et al., 2006Jirovetz, Eller, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1Methyl SiliconeHP-5OV-101CP Sil 5 CB
Column length (m)  25.30.25.30.
Carrier gas HeliumHeHeliumHeN2
Substrate      
Column diameter (mm)  0.250.320.250.32
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.90.60.100.50.
Tend (C) 220.220.260.250.300.
Heat rate (K/min) 5.7.5.8.4.
Initial hold (min)  2.2.  
Final hold (min) 6. 13.  
I 1240.1260.1257.1238.1226.
ReferenceKiran, Bhavani, et al., 2006Kitchlu, Bakshi, et al., 2006Kucuk, Gulec, et al., 2006Lattoo, Dhar, et al., 2006Lis and Milczarek, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101HP-5DB-5CP-Sil 5 CBNB-30
Column length (m) 25.30.30.25.30.
Carrier gas HeHeliumHeHydrogenHe
Substrate      
Column diameter (mm) 0.20.320.250.250.2
Phase thickness (μm) 0.20.250.250.150.25
Tstart (C) 70.40.60.50.50.
Tend (C) 200.240.220.230.250.
Heat rate (K/min) 3.4.4.3.2.
Initial hold (min) 2. 5.  
Final hold (min) 15.5.   
I 1264.1253.1256.1233.1240.
ReferenceMastelic, Jerkovic, et al., 2006Miyazawa and Kawata, 2006Morteza-Semnani K., Saeedi M., et al., 2006Olawore, Usman, et al., 2006Orav, Raal, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5PE-5SPB-5DB-5
Column length (m) 25.30.50.30.30.
Carrier gas N2HeHeHeliumHydrogen
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.150.250.250.250.25
Tstart (C) 50.60.100.60.70.
Tend (C) 200.280.280.250.280.
Heat rate (K/min) 4.5.3.4.4.
Initial hold (min) 3.0.51.2.4.
Final hold (min)  2. 20. 
I 1260.1276.1259.1254.1256.
ReferenceOuamba, Ouabonzi, et al., 2006Ozel, Gogus, et al., 2006Pandey-Rai S., Mallavarapu G.R., et al., 2006Pino, Marquez, et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1HP-5MSDB-5HP-5 MS
Column length (m) 30.60.30.30.30.
Carrier gas   HeH2Helium
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm) 0.250.250.250.180.25
Tstart (C) 50.70.60.60.60.
Tend (C) 250.230.280.240.250.
Heat rate (K/min) 10.2.3.3.2.
Initial hold (min) 5.2.5. 8.
Final hold (min)  20.  15.
I 1254.1239.1256.1257.1250.
ReferenceRobinson, 2006Sawamura, Onishi, et al., 2006Setzer, Noletto, et al., 2006Silva, Oliveira, et al., 2006Tigrine-Kordiani, Meklati, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1Methyl SiliconeHP-5BPX-5SPB-1
Column length (m) 30.25.30.50.50.
Carrier gas  N2He He
Substrate      
Column diameter (mm) 0.320.30.250.220.2
Phase thickness (μm) 0.250.150.251.0.33
Tstart (C) 60.50.60.70.50.
Tend (C) 230.210.250.280.220.
Heat rate (K/min) 3.2.10.4.4.
Initial hold (min) 3.5.2. 1.
Final hold (min) 10. 10.4.10.
I 1244.1267.1260.1268.1235.
ReferenceTohar, Mohd, et al., 2006Tonzibo, Coffy, et al., 2006Wang, Yang, et al., 2006Wohlmuth, Smith, et al., 2006Wong, Lim, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5DB-5SPB-5BPX-5
Column length (m) 30.30.50.60.25.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.30.320.22
Phase thickness (μm) 0.250.250.251.0.25
Tstart (C) 50.40.60.40.50.
Tend (C) 250.250.240.230.320.
Heat rate (K/min) 4.4.2.3.5.
Initial hold (min) 1.  5.5.
Final hold (min) 10.    
I 1236.1242.1252.1258.1261.
ReferenceWong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006Chagonda and Chalchat, 2005Cornu, Kondjoyan, et al., 2005Dickschat, Martens, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RSL-200SPB-5RTX-5 MSHP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.20.250.530.250.25
Phase thickness (μm) 0.330.25 0.250.25
Tstart (C) 60.40.100.50.60.
Tend (C) 240.280.250.280.280.
Heat rate (K/min) 3.6.5.8.3.
Initial hold (min)  2. 2.5.
Final hold (min) 7.10. 2. 
I 1254.1252.1263.1261.1255.
ReferenceDuarte, Figueira, et al., 2005Jirovetz, Buchbauer, et al., 2005Kilic, Kollmannsberger, et al., 2005Pellati, Benvenuti, et al., 2005Setzer, Noletto, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSHP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.40.
Tend (C) 280.240.285.280.220.
Heat rate (K/min) 3.3.4.33.3.
Initial hold (min)  3.  5.
Final hold (min)     10.
I 1260.1301.1255.1226.1245.
ReferenceSlavkovska, Couladis, et al., 2005Tepe B., Sokmen M., et al., 2005Tesevic, Nikicevic, et al., 2005Tzakou, Bazos, et al., 2005Vichi, Riu-Aumatell, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1DB-5DB-5DB-5MS
Column length (m) 50.50.25.60.30.
Carrier gas HeHeNitrogenHeHe
Substrate      
Column diameter (mm) 0.20.20.250.250.25
Phase thickness (μm) 0.330.330.250.250.25
Tstart (C) 50.50.60.40.60.
Tend (C) 220.220.240.280.240.
Heat rate (K/min) 4.4.3.4.3.
Initial hold (min) 3.3. 4. 
Final hold (min) 30.30.   
I 1233.1235.1254.1255.1257.
ReferenceWong, Lee, et al., 2005Wong and Tan, 2005JAvidnia, Mojab, et al., 2004Kalvandi, Sefidkon, et al., 2004paz Lima, Silva, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5MSNB-30NB-30DB-1
Column length (m) 30.30.50.50.60.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.320.250.20.200.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.70.
Tend (C) 300.280.250.250.230.
Heat rate (K/min) 4.3.2.2.2.
Initial hold (min)     2.
Final hold (min)     20.
I 1236.1255.1242.1242.1241.
ReferenceLis, Boczek, et al., 2004Mimica-Dukic, Bozin, et al., 2004Raal, Arak, et al., 2004Raal, Paaver, et al., 2004Sawamura, Son, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-1HP-1DB-1
Column length (m) 60.25.60.30.30.
Carrier gas NitrogenH2HeHeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.520.250.250.25
Tstart (C) 70.40.70.70.50.
Tend (C) 230.240.230.200.200.
Heat rate (K/min) 2.4.2.10.5.
Initial hold (min) 2. 2.  
Final hold (min)   20.  
I 1241.1253.1241.1249.1220.
ReferenceSawamura, Sou, et al., 2004Simic, Sokovic, et al., 2004Choi, 2003Fekam Boyom, Amvam Zollo, et al., 2003Fekam Boyom, Ngouana, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSRSL-200RSL-200RSL-200DB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeH2H2H2He
Substrate      
Column diameter (mm) 0.250.320.250.320.2
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.40.50.
Tend (C) 275.280.280.280.220.
Heat rate (K/min) 4.6.6.6.3.
Initial hold (min)  5.2.5.2.
Final hold (min)  5.10.5.10.
I 1253.1241.1252.1242.1258.
ReferenceGhannadi, Aghazari, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Jirovetz, Buchbauer, et al., 2003, 3Juteau, Jerkovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1ZB-1OV-101MPS-5DB-5
Column length (m) 30.30.12. 30.
Carrier gas N2N2  He
Substrate      
Column diameter (mm) 0.250.250.32 0.25
Phase thickness (μm) 0.250.250.32 0.25
Tstart (C) 80.45.35.70.60.
Tend (C) 250.230.225.180.240.
Heat rate (K/min) 4.3.6.5.3.
Initial hold (min)   3.2. 
Final hold (min)      
I 1233.1234.1240.1253.1255.
ReferenceMahalwal and Ali, 2003Mierendorff, Stahl-Biskup, et al., 2003Murakami, Goldstein, et al., 2003Nakahara, Alzoreky, et al., 2003da Silva, Luz, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-1DB-1CP Sil 5 CB
Column length (m) 60.60.60.60.25.
Carrier gas   N2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.4
Tstart (C) 40.40.70.70.60.
Tend (C) 250.250.230.230.260.
Heat rate (K/min) 5.5.2.2.5.
Initial hold (min) 15.15.2.2. 
Final hold (min)   20.20.40.
I 1255.1254.1246.1243.1238.
ReferenceStashenko, Jaramillo, et al., 2003Stashenko, Jaramillo, et al., 2003Tu, Onishi, et al., 2003Tu, Onishi, et al., 2003, 2Azaz. D., Demirci, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-1BP-1DB-5HP-5
Column length (m) 30.60.25.30.30.
Carrier gas HeHeN2N2N2
Substrate      
Column diameter (mm) 0.250.320.500.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 75.50.60.50.50.
Tend (C) 200.200.220.250.250.
Heat rate (K/min) 3.3.5.4.4.
Initial hold (min) 4.6.  5.
Final hold (min) 8. 10.  
I 1253.1242.1240.1255.1256.
ReferenceCicció and Gómez-Laurito, 2002Cimanga, Apers, et al., 2002Das, Ram, et al., 2002Farah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5SE-30DB-5DB-5MS
Column length (m) 30.30.50.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.70.60.60.
Tend (C) 245.275.240.240.240.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min) 20.    
Final hold (min)      
I 1240.1253.1245.1254.1254.
ReferenceGancel, Ollé, et al., 2002Ghannadi, Sajjadi, et al., 2002Iñigo, Palá-Paúl, et al., 2002Kobaisy, Tellez, et al., 2002Maia, Zoghbi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5DB-1BP-5BP-1
Column length (m) 50.30.60.50.30.
Carrier gas N2HeliumHeH2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.251.0.25
Tstart (C) 80.60.40.60.60.
Tend (C) 225.250.280.270.220.
Heat rate (K/min) 4.4.4.6.5.
Initial hold (min)  2.5.  
Final hold (min)  20.   
I 1228.1255.1230.1274.1241.
ReferencePalá-Paúl, Pérez-Alonso, et al., 2002Pino, Marbot, et al., 2002Sefidkon, Jalili, et al., 2002Doimo, 2001Gupta, Mallavarapu, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1BP-1HP-5 MSPTE-5
Column length (m) 30.30.50.30.60.
Carrier gas N2N2HeHeliumH2
Substrate      
Column diameter (mm) 0.250.250.220.250.32
Phase thickness (μm) 0.250.250.250.250.3
Tstart (C) 70.70.60.50.60.
Tend (C) 180.180.230.250.285.
Heat rate (K/min) 2.2.2.5.4.3
Initial hold (min) 2.2. 2. 
Final hold (min) 1.1.35.5. 
I 1237.1245.1232.1245.1255.
ReferenceKamath, Asha, et al., 2001Kamath, Asha, et al., 2001Lota, de Rocca Serra, et al., 2001Shang, Hu, et al., 2001Stojanovic, Palic, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101RSL-200SPB-5DB-1DB-5
Column length (m) 50.60.60.25.30.
Carrier gas N2H2HeNitrogenN2
Substrate      
Column diameter (mm) 0.250.320.250.500.22
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 80.40.70.60.70.
Tend (C) 200.250.240.220.230.
Heat rate (K/min) 2.6.5.5.4.
Initial hold (min)   8. 2.
Final hold (min)   20. 20.
I 1246.1238.1260.1239.1251.
ReferenceYang, 2001Jirovetz, Puschmann, et al., 2000Kim, Kim, et al., 2000Mallavarapu, Rao, et al., 2000Mitiku, Sawamura, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SE-30BP-5HP-1BP-1
Column length (m) 50.25.50.25.25.
Carrier gas NitrogenHeHeH2N2
Substrate      
Column diameter (mm) 0.250.20.320.320.50
Phase thickness (μm)   1.0.170.25
Tstart (C) 40.60.40.40.60.
Tend (C) 200.230.190.260.220.
Heat rate (K/min) 2.3.2.3.5.
Initial hold (min) 10. 5.5. 
Final hold (min)     10.
I 1243.1242.1267.1234.1238.
ReferenceTamura, Boonbumrung, et al., 2000Ali N.A.M. and Jantan, 1999Lopez, Ferreira, et al., 1999Lopes, Koketsu, et al., 1999Mallavarapu, Kulkarni, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5SE-30OV-1HP-1
Column length (m) 50.30.25.25.25.
Carrier gas N2HeHeH2 
Substrate      
Column diameter (mm) 0.20.250.20.250.20
Phase thickness (μm)    0.25 
Tstart (C) 80.40.60.40.35.
Tend (C) 200.230.230.220.250.
Heat rate (K/min) 1.4.3.3.4.
Initial hold (min)  1.10.5. 
Final hold (min) 20.  5. 
I 1241.1250.1242.1235.1230.
ReferenceMenon, Chacko, et al., 1999Mockute and Bernotiene, 1999Mohd and Jantan, 1999Oberhofer, Nikiforov, et al., 1999Ong and Acree, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1OV-101CP Sil 5 CBDB-5MS
Column length (m) 25.60.25.25.30.
Carrier gas N2HeNitrogenN2He
Substrate      
Column diameter (mm) 0.50.250.20 0.25
Phase thickness (μm)  0.25 0.390.25
Tstart (C) 60.40.60.60.60.
Tend (C) 220.280.220.220.240.
Heat rate (K/min) 5.4.4.5.3.
Initial hold (min)  5.0.  
Final hold (min) 10. 0.  
I 1238.1239.1252.1237.1253.
ReferenceRao, Bhattacharya, et al., 1999Sefidkon, Dabiri, et al., 1999Tropnikova, Zenkevich, et al., 1999Weyerstahl, Marschall, et al., 1999Zoghbi, Andrade, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30CBP-1HP-1HP-5CP Sil 5 CB
Column length (m) 25.30.25.25.25.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.20.250.320.20.25
Phase thickness (μm)    0.330.25
Tstart (C) 60.60.35.70.60.
Tend (C) 180.240.250.290.300.
Heat rate (K/min) 3.4.4.3.6.
Initial hold (min) 10.  8. 
Final hold (min)    20. 
I 1234.1242.1230.1258.1233.
ReferenceJantan, Ahmad, et al., 1998Lamarque, Maestri, et al., 1998Ong and Acree, 1998Poiana, Sicari, et al., 1998Bos, Woerdenbag, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101BP-1BP-1BP-1DB-1
Column length (m) 50.25.25.25.60.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.250.500.500.500.32
Phase thickness (μm)     0.50
Tstart (C) 50.60.60.60.50.
Tend (C) 250.220.220.220.250.
Heat rate (K/min) 2.5.5.5.8.
Initial hold (min)     1.
Final hold (min)     6.
I 1228.1241.1241.1242.1243.
ReferenceOrav, Kailas, et al., 1996Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996Sagrero-Nieves and Bartley, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1OV-101OV-101DB-1DB-1
Column length (m) 50.15.52.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.320.260.250.25
Phase thickness (μm) 0.33  0.250.25
Tstart (C) 40.35.50.70.70.
Tend (C) 200.250.220.270.270.
Heat rate (K/min) 3.6.3.2.52.5
Initial hold (min) 3.3. 5.5.
Final hold (min) 30.    
I 1232.1241.1250.1237.1237.
ReferenceWong and Lai, 1996Chisholm, Guiher, et al., 1995Dzumayev, Tsibulskaya, et al., 1995Tirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-101DB-5DB-5OV-101
Column length (m) 30.50.30.30.50.
Carrier gas HeliumH2H2H2 
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm)  0.31.1. 
Tstart (C) 50.65.40.40.80.
Tend (C) 250.300.220.220.200.
Heat rate (K/min) 4.2.3.3.2.
Initial hold (min)  5.   
Final hold (min)      
I 1221.1236.1258.1259.1236.
ReferenceGomez and Ledbetter, 1994Demarne and van der Walt, 1993Moio, Dekimpe, et al., 1993Moio, Dekimpe, et al., 1993Tamura, Yang, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-1DB-1DB-1
Column length (m) 50.60.60.60.30.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.250.320.250.25 
Phase thickness (μm)  1.20.250.25 
Tstart (C) 80.30.50.50.80.
Tend (C) 200.240.240.240.220.
Heat rate (K/min) 2.3.3.3.4.
Initial hold (min)  10.   
Final hold (min)      
I 1236.1296.1236.1239.1230.
ReferenceTamura, Yang, et al., 1993Ciccioli, Cecinato, et al., 1992Shiota, 1991Shiota, 1991Velasco-Negueruela, Pérez Alonso, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101OV-101OV-101SE-54
Column length (m) 60.50.50.50.25.
Carrier gas  N2N2N2N2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm)      
Tstart (C) 50.80.80.80.60.
Tend (C) 250.200.200.200.260.
Heat rate (K/min) 4.2.2.2.6.
Initial hold (min) 0.1   2.
Final hold (min) 5.    
I 1234.1234.1235.1236.1255.
ReferenceBinder and Flath, 1989Sugisawa, Yamamoto, et al., 1989Sugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Bestmann, Classen, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-101DB-1
Column length (m) 30.60.
Carrier gas He 
Substrate   
Column diameter (mm) 0.50.32
Phase thickness (μm) 0.8 
Tstart (C) 40.50.
Tend (C) 220.250.
Heat rate (K/min) 2.4.
Initial hold (min)  0.1
Final hold (min)  5.
I 1238.1233.
ReferenceDe Pooter and Schamp, 1986Flath, Mon, et al., 1983
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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