Citronellol

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Normal alkane RI, polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxVF-Wax MSBP-20TC-WaxInnowax
Column length (m) 60.60. 60.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.220.25 0.250.25
Phase thickness (μm) 0.250.25  0.25
Tstart (C) 60.60.60.40.40.
Tend (C) 230.220.200.230.250.
Heat rate (K/min) 2.3.5.3.6.
Initial hold (min)  5. 3.1.
Final hold (min) 5.25.  4.
I 1724.1760.1740.1763.1777.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Duarte, Dias, et al., 2010Mishra, Chaudhary, et al., 2010Miyazawa, Fujita, et al., 2010Seo, Kim, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP-InnowaxHP-InnowaxCarbowaxCarbowax
Column length (m) 30.50.30.60.60.
Carrier gas HeliumHeliumN2HeHe
Substrate      
Column diameter (mm) 0.250.200.250.20.25
Phase thickness (μm) 0.250.200.250.250.25
Tstart (C) 40.45.50.60.40.
Tend (C) 230.190.240.250.180.
Heat rate (K/min) 3.4.5.2.5.
Initial hold (min) 2.2.1.8. 
Final hold (min) 5.50.4.15. 
I 1764.1766.1764.1749.1718.
ReferenceZhao, Xu, et al., 2009Soria, Sanz, et al., 2008Cheraif, Ben Jannet, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Singh, Kumar, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10DB-WaxBP-20Supelcowax 10
Column length (m) 30.30.60.50.30.
Carrier gas  HeHe Helium
Substrate      
Column diameter (mm) 0.250.250.250.220.20
Phase thickness (μm) 0.250.250.250.250.20
Tstart (C) 40.40.60.60.70.
Tend (C) 250.250.180.220.220.
Heat rate (K/min) 2.3.3.2.3.
Initial hold (min)  5.8.  
Final hold (min) 33.10.80.20.15.
I 1778.1780.1773.1763.1764.
ReferenceSylvestre, Pichette, et al., 2007Vichi, Riu-Aumatell, et al., 2007Wei A. and Shibamoto T., 2007Boti, Yao, et al., 2006Cavaleiro, Pinto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxBP-20DB-Wax EtrDB-WaxDB-Wax
Column length (m) 60.50.60.60.60.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.60.40.70.70.
Tend (C) 230.220.230.230.230.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min) 2. 5.2.2.
Final hold (min) 20.20.100.20.20.
I 1774.1764.1775.1764.1763.
ReferenceChoi H.S., 2006Fanciullino, Tomi, et al., 2006Ibarz, Ferreira, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-20MCarbowax 20MStabilwaxStabilwaxInnowax
Column length (m) 30.60.30.30.60.
Carrier gas HeN2H2 He
Substrate      
Column diameter (mm) 0.20.250.320.320.25
Phase thickness (μm) 0.250.250.50.50.25
Tstart (C) 50.40.40.40.60.
Tend (C) 250.190.280.280.240.
Heat rate (K/min) 2.10.6.6.5.
Initial hold (min)  2.5.5. 
Final hold (min)  15.5.5.30.
I 1800.1722.1777.1777.1763.
ReferenceOrav, Raal, et al., 2006Babu and Kaul, 2005Jirovetz, Buchbauer, et al., 2005Jirovetz, Buchbauer, et al., 2005, 2Joichi, Yomogida, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxPE-WaxSupelcowax-10
Column length (m) 30.60.60.50.30.
Carrier gas HeN2NitrogenH2 
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.500.250.25
Tstart (C) 50.70.35.60.40.
Tend (C) 180.230.235.220.220.
Heat rate (K/min) 3.2.2.4.3.
Initial hold (min)  2.4. 5.
Final hold (min) 40.20.30.2.10.
I 1761.1775.1791.1779.1780.
ReferenceLee, Umano, et al., 2005Njoroge, Koaze, et al., 2005Qian and Wang, 2005Ram, Kumar, et al., 2005Vichi, Riu-Aumatell, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 30.60.60.60.60.
Carrier gas HeN2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25  
Tstart (C) 90.70.70.60.60.
Tend (C) 220.230.230.220.220.
Heat rate (K/min) 7.2.2.2.2.
Initial hold (min) 2.2.2.4.4.
Final hold (min) 5.20.20.  
I 1803.1772.1774.1765.1765.
ReferenceAgnihotri, Thappa, et al., 2004Choi, 2004Choi, 2004, 2Jiang and Kubota, 2004Jiang and Kubota, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-20MDB-WaxDB-WaxDB-WaxPEG 20M
Column length (m) 50.60.60.60. 
Carrier gas He NitrogenHelium 
Substrate      
Column diameter (mm) 0.20.250.250.25 
Phase thickness (μm) 0.250.250.25  
Tstart (C) 50.70.70.70.70.
Tend (C) 250.230.230.210.180.
Heat rate (K/min) 2.2.2.2.5.
Initial hold (min)  2.2. 2.
Final hold (min)  20. 60. 
I 1800.1775.1775.1766.1755.
ReferenceRaal, Arak, et al., 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Mookdasanit, Tamura, et al., 2003Nakahara, Alzoreky, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.60.60.60.60.
Carrier gas N2N2H2N2N2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.40.70.70.
Tend (C) 230.230.245.230.230.
Heat rate (K/min) 2.2.1.52.2.
Initial hold (min) 2.2. 2. 
Final hold (min) 20.20.20.20. 
I 1745.1752.1764.1757.1771.
ReferenceTu, Onishi, et al., 2003Tu, Onishi, et al., 2003, 2Gancel, Ollé, et al., 2002Tu, Onishi, et al., 2002Tu, Thanh, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.60.30.60.60.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.5  
Tstart (C) 40.45.40.60.40.
Tend (C) 200.240.200.220.220.
Heat rate (K/min) 2.3.4.2.2.
Initial hold (min) 2. 5.4. 
Final hold (min)   60.  
I 1759.1766.1786.1789.1782.
ReferenceUmano, Hagi, et al., 2002Christoph, 2001Ferreira, Aznar, et al., 2001Jiang, Kojima, et al., 2001Jiang and Kubota, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20Supelcowax-10Supelcowax-10DB-WaxSupelcowax-10
Column length (m) 50.30.60.60.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.220.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.70.60.40.60.
Tend (C) 230.240.280.200.220.
Heat rate (K/min) 2.5.4.2.4.
Initial hold (min)  8. 2. 
Final hold (min) 35.20.   
I 1756.1755.1740.1769.1752.
ReferenceLota, de Rocca Serra, et al., 2001Kim, Kim, et al., 2000Korány, Mednyánszky, et al., 2000Umano, Hagi, et al., 2000Choo, Wong, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxDB-WaxCP-Wax 52CBCarbowax 20MDB-Wax
Column length (m) 25.60.25.60.30.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm)  0.250.20.50.25
Tstart (C) 35.40.60.40.45.
Tend (C) 250.200.240.190.220.
Heat rate (K/min) 4.2.6.2.3.
Initial hold (min)  2.2.5. 
Final hold (min)   10.  
I 1764.1768.1771.1773.1778.
ReferenceOng and Acree, 1999Umano, Nakahara, et al., 1999Chisowa, Hall, et al., 1998Ferreira, Ardanuy, et al., 1998Mölleken, Sinnwell, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxDB-WaxPEG-20MPEG-20MSupelcowax-10
Column length (m) 25.60.60.50.60.
Carrier gas  H2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm)  0.25  0.25
Tstart (C) 35.60.70.70.40.
Tend (C) 250.220.210.250.200.
Heat rate (K/min) 4.3.3.2.3.
Initial hold (min)     3.
Final hold (min)     30.
I 1764.1760.1763.1764.1768.
ReferenceOng and Acree, 1998Werkhoff, Güntert, et al., 1998Awano, Honda, et al., 1997Orav, Kailas, et al., 1996Wong and Lai, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedPacked
Active phase Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 60.100.100.2.2.
Carrier gas He  HydrogenHydrogen
Substrate    Gas-Chrom Z (80-100 mesh)Gas-Chrom Z (80-100 mesh)
Column diameter (mm) 0.250.250.25  
Phase thickness (μm) 0.25    
Tstart (C) 50.70.70.65.65.
Tend (C) 150.170.170.220.220.
Heat rate (K/min) 2.1.1.4.4.
Initial hold (min) 10.    
Final hold (min) 20.    
I 1751.1744.1745.1741.1741.
ReferenceTirado, Stashenko, et al., 1995Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977Stancher and Pertoldi, 1967Stancher and Pertoldi, 1967
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

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Mishra, Chaudhary, et al., 2010
Mishra, R.K.; Chaudhary, S.; Pandey, R.; Gupta, S.; Mallavarapu, G.R.; Kumar, S., Analysis of linalool content in the inflorescence (flower) essential oil and leaf oil of Lippia alba cultivar Kavach, J. Essen. Oil Res., 2010, 22, 1, 3-7, https://doi.org/10.1080/10412905.2010.9700253 . [all data]

Miyazawa, Fujita, et al., 2010
Miyazawa, N.; Fujita, A.; Kubota, K., Aroma character impact compounds in Kinokuni Mandarin Orange (Citrus kinikuni) compared with Satsuma Mandarin Orange, Biosci. Biotechnol. Biochem., 2010, 74, 4, 835-842, https://doi.org/10.1271/bbb.90937 . [all data]

Seo, Kim, et al., 2009
Seo, S.-M.; Kim, J.; Lee, S.-G.; Shin, C.-H.; Shin, S.-C.; Park, I.-K., Fumigant antitermitic activity of plant essential oils and components from Aiowan (Trachyspermum ammi), Allspice (Pimenta dioica), Caraway (Carum carvi), Dill (Anethum graveolens), Geranium (Pelargonium graveolens), and Litsea (Litsea cubeba( oils against Japanese termite (Reticulitermes speratus Kolbe), J. Agric. Food Chem., 2009, 57, 15, 6596-6602. [all data]

Zhao, Xu, et al., 2009
Zhao, Y.; Xu, Y.; Li, J.; Fan, W.; Jiang, W., Profile of volatile compounds in 11 brandies by headspace solid-phase microextraction followed by gas chromatography-mass spectrometry, J. Food. Sci., 2009, 74, 2, c90-c99, https://doi.org/10.1111/j.1750-3841.2008.01029.x . [all data]

Soria, Sanz, et al., 2008
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Cheraif, Ben Jannet, et al., 2007
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Ferhat, Tigrine-Kordjani, et al., 2007
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Singh, Kumar, et al., 2007
Singh, B.; Kumar, R.; Bhandari, S.; Pathania, S.; Lal, B., Volatile constituents of natural Boswellia serrata oleo-gum-resin and commercial samples, Flavour Fragr. J., 2007, 22, 2, 145-147, https://doi.org/10.1002/ffj.1772 . [all data]

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Sylvestre, M.; Pichette, A.; Longtin, A.; Martin, M.-A.C.; Bercion, S.R.; Legault, J., Chemical composition of leaf essential oil of Hedyosmum arborescens and evaluation of its anticancer activity, Natural Product Communications, 2007, 2, 12, 1269-1272. [all data]

Vichi, Riu-Aumatell, et al., 2007
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Wei A. and Shibamoto T., 2007
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Boti, Yao, et al., 2006
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Cavaleiro, Pinto, et al., 2006
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Choi H.S., 2006
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Lan Phi N.T., Nishiyama C., et al., 2006
Lan Phi N.T.; Nishiyama C.; Choi H.-S.; Sawamura M., Evaluation of aroma characteristic compounds of Citrus natsudaidai Hayata (Natsudaidai) cold-pressed peel oil, Biosci. Biotechnol. Biochem., 2006, 70, 8, 1832-1838, https://doi.org/10.1271/bbb.50705 . [all data]

Orav, Raal, et al., 2006
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Jirovetz, Buchbauer, et al., 2005
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Jirovetz, Buchbauer, et al., 2005, 2
Jirovetz, L.; Buchbauer, G.; Stoyanova, A.; Balinova, A.; Guangjiun, Z.; Xihan, M., Solid phase microextraction/gas chromatographic and olfactory analysis of the scent and fixative properties of the essential oil of Rosa damascena L. from China, Flavour Fragr. J., 2005, 20, 1, 7-12, https://doi.org/10.1002/ffj.1375 . [all data]

Joichi, Yomogida, et al., 2005
Joichi, A.; Yomogida, K.; Awano, K.; Ueda, Y., Volatile components of tea-scented modern roses and ancient Chinese roses, Flavour Fragr. J., 2005, 20, 2, 152-157, https://doi.org/10.1002/ffj.1388 . [all data]

Lee, Umano, et al., 2005
Lee, S.-J.; Umano, K.; Shibamoto, T.; Lee, K.-G., Identification of volatile components in basil (Ocimum basilicum L.) and thyme leaves (Thymus vulgaris L.) and their antioxidant properties, Food Chem., 2005, 91, 1, 131-137, https://doi.org/10.1016/j.foodchem.2004.05.056 . [all data]

Njoroge, Koaze, et al., 2005
Njoroge, S.M.; Koaze, H.; Mwaniki, M.; Minh Tu, N.T.; Sawamura, M., Essential oils of Kenyan Citrus fruits: volatile components of two varieties of mandarins (Citrus reticulata) and a tangelo (C. paradisi × C. tangerina), Flavour Fragr. J., 2005, 20, 1, 74-79, https://doi.org/10.1002/ffj.1376 . [all data]

Qian and Wang, 2005
Qian, M.C.; Wang, Y., Seasonal Variations of Volatile Composition and Odor Activity Value of Marion (Rubus spp. hyb) and Thornless Evergreen (R.laciniatus L.) Blackberries, J. Food. Sci., 2005, 70, 1, c13-c20, https://doi.org/10.1111/j.1365-2621.2005.tb09013.x . [all data]

Ram, Kumar, et al., 2005
Ram, P.; Kumar, B.; Naqvi, A.A.; Verma, R.S.; Patra, N.K., Post-harvest storage effect on quantity and quality of rose-scented geranium (Pelargonium sp. cv. 'Bourbon') oil in Uttaranchal, Flavour Fragr. J., 2005, 20, 6, 666-668, https://doi.org/10.1002/ffj.1544 . [all data]

Vichi, Riu-Aumatell, et al., 2005
Vichi, S.; Riu-Aumatell, M.; Mora-Pons, M.; Buxaderas, S.; Lopez-Tamames, E., Characterization of Volatiles in Different Dry Gins, J. Agric. Food Chem., 2005, 53, 26, 10154-10160, https://doi.org/10.1021/jf058121b . [all data]

Agnihotri, Thappa, et al., 2004
Agnihotri, V.K.; Thappa, R.K.; Meena, B.; Kapahi, B.K.; Saxena, R.K.; Qazi, G.N.; Agarwal, S.G., Essential oil composition of aerial parts of Angelica glauca growing wild in North-West Himalaya (India), Phytochemistry, 2004, 65, 16, 2411-2413, https://doi.org/10.1016/j.phytochem.2004.07.004 . [all data]

Choi, 2004
Choi, H.-S., Volatile constituents of satsuma mandarins growing in Korea, Flavour Fragr. J., 2004, 19, 5, 406-412, https://doi.org/10.1002/ffj.1283 . [all data]

Choi, 2004, 2
Choi, H.-S., Aroma evaluation of an aquatic herb, changpo (Acorus calamus Var. angustatus Bess), by AEDA and SPME, J. Agric. Food Chem., 2004, 52, 26, 8099-8104, https://doi.org/10.1021/jf040239p . [all data]

Jiang and Kubota, 2004
Jiang, L.; Kubota, K., Differences in the volatile components and their odor characteristics of green and ripe fruits and dried pericarp of Japanese pepper (Xanthoxylum piperitum DC.), J. Agric. Food Chem., 2004, 52, 13, 4197-4203, https://doi.org/10.1021/jf030663a . [all data]

Raal, Arak, et al., 2004
Raal, A.; Arak, E.; Orav, A., Chemical composition of coriander seed essential oil and their conformity with EP standards, Agraarteadus, 2004, 15, 4, 234-239. [all data]

Sawamura, Son, et al., 2004
Sawamura, M.; Son, U.-S.; Choi, H.-S.; Kim, M.-S.L.; Phi, N.T.L.; Fears, M.; Kumagai, Compositional changes in commercial lemon essential oil for aromatherapy, Int. J. Aromatherapy, 2004, 14, 1, 27-36, https://doi.org/10.1016/j.ijat.2004.02.001 . [all data]

Sawamura, Sou, et al., 2004
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Notes

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