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ClCH2C(O)OCH(CH3)2

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSOV-101
Column length (m) 25.25.25.
Carrier gas HeliumHeliumNitrogen
Substrate    
Column diameter (mm) 0.200.200.20
Phase thickness (mum) 0.330.330.25
Tstart (C) 45.45.40.
Tend (C) 280.280.220.
Heat rate (K/min) 5.5.6.
Initial hold (min) 1.1. 
Final hold (min) 2.2. 
I 850.880.861.
ReferenceKornilova, Ukolov, et al., 2012Kornilova, Ukolov, et al., 2012Zenkevich, Eliseenkov, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kornilova, Ukolov, et al., 2012
Kornilova, T.A.; Ukolov, A.I.; Kostikov, R.R.; Zenkevich, I.G., Stability of diazocarbonyl compounds under the conditions of gas chromatography and chromatography-mass spectrometry analysis, Rus. J. General Chem., 2012, 82, 10, 1675-1685, https://doi.org/10.1134/S1070363212100088 . [all data]

Zenkevich, Eliseenkov, et al., 2011
Zenkevich, I.G.; Eliseenkov, E.V.; Kasatochkin, A.N.; Ukolov, A.I., Identification of the products of nonregioselective organic reactions by chromatography - mass spectrometry: chloro derivatives of dialkyl ethers, Rus. J. Anal. Chem., 2011, 66, 14, 1445-1454, https://doi.org/10.1134/S1061934811140218 . [all data]


Notes

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