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2-Propenal, 3-phenyl-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSBPX-5BPX-5BPX-5BPX-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHydrogenHydrogenHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.100.60.60.60.
Tend (C) 230.999.999.999.999.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)      
Final hold (min)      
I 1278.1303.1295.1296.1297.
ReferencePripdeevech and Saansoomchai, 2013Bieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5BPX-5Equity-5 MSHP-1HP-1
Column length (m) 30.30.30.30.50.
Carrier gas HydrogenHydrogenHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 60.60.40.70.60.
Tend (C) 999.999.260.200.250.
Heat rate (K/min) 3.5.1.510.2.
Initial hold (min)     4.
Final hold (min)     30.
I 1301.1300.1273.1251.1231.
ReferenceBieri and Marriott, 2008Bieri and Marriott, 2008Mondello, Casilli, et al., 2008Dongmo, Tatsadjieu, et al., 2007Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase FSOT-RSL-200DB-5HP-1HP-5DB-1
Column length (m) 30.30.50.30.60.
Carrier gas HydrogenHe HeliumHe
Substrate      
Column diameter (mm) 0.320.250.20.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.40.35.
Tend (C) 280.250.250.250.230.
Heat rate (K/min) 6.4.2.5.2.
Initial hold (min) 5.2.60.2.4.
Final hold (min) 5.10. 5.25.
I 1259.1260.1235.1250.1222.
ReferenceSchmidt, Jirovetz, et al., 2006Shen X., Gao Y., et al., 2006Fernandez, Lizzani-Cuvelier, et al., 2005N/APark, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1CP Sil 8 CBOV-101
Column length (m) 60.60.60.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.320.320.250.22
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 35.35.35.50.80.
Tend (C) 230.230.230.200.200.
Heat rate (K/min) 2.2.2.10.2.
Initial hold (min) 4.4.4.3. 
Final hold (min) 25.25.25.2. 
I 1223.1223.1227.1252.1250.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Wang and Guo-Y. -L., 2004Egolf and Jurs, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase Ultra-1
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum) 0.25
Tstart (C) 80.
Tend (C) 260.
Heat rate (K/min) 3.
Initial hold (min)  
Final hold (min)  
I 1223.
ReferenceOkumura, 1991
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pripdeevech and Saansoomchai, 2013
Pripdeevech, P.; Saansoomchai, J., Antibacterial activity and chemical composition of essential oil and various extracts of Fagraea fragrans Roxb. flowers, Chiang Mai J. Sci., 2013, 40, 2, 214-223. [all data]

Bieri and Marriott, 2008
Bieri, S.; Marriott, P.J., Dual-injection system with multiply injections for determining sidimentional retention indexes in comprehensive two-dimensional gas chromatography, Anal. Chem., 2008, 80, 3, 760-768, https://doi.org/10.1021/ac071367q . [all data]

Mondello, Casilli, et al., 2008
Mondello, L.; Casilli, A.; Tranchida, Q.; Sciarrone, D.; Dugo, P.; Dugo, G., Analysis of allergens in fragrances using multiple heart-cut multidimentional gas chromatography - mass spectrometry, LC-GC Europe, 2008, 21, 130. [all data]

Dongmo, Tatsadjieu, et al., 2007
Dongmo, P.M.J.; Tatsadjieu, L.N.; Tchoumbougnang, F.; Sameza, M.L.; Dongmo, B.N.; Zollo, P.H.A.; Menut, C., Chemical composition, antiradical and antifungal activities os eeesntioal oil af the leaves of Cinnamomum zeylanicum Blume from Cameroon, Natural Product Communications, 2007, 2, 12, 1287-1290. [all data]

Castel, Fernandez, et al., 2006
Castel, C.; Fernandez, X.; Lizzani-Cuvelier, L.; Perichet, C.; Lavoine, S., Characterization of the Chemical Composition of a Byproduct from Siam Benzoin Gum, J. Agric. Food Chem., 2006, 54, 23, 8848-8854, https://doi.org/10.1021/jf061193y . [all data]

Schmidt, Jirovetz, et al., 2006
Schmidt, E.; Jirovetz, L.; Buchbauer, G.; Eller, G.A.; Stoilova, I.; Krastanov, A.; Stoyanova, A.; Geisseler, M., Composition and antioxidant activities of the essential oil of cinnamon (Cinnamomum zeylanicum Blume) leaves from Sri Lanka, Jeobp, 2006, 9, 2, 170-182. [all data]

Shen X., Gao Y., et al., 2006
Shen X.; Gao Y.; Su Q.D., Constituents of the essential oil of Rhizoma polygonati, Flavour Fragr. J., 2006, 21, 3, 556-558, https://doi.org/10.1002/ffj.1666 . [all data]

Fernandez, Lizzani-Cuvelier, et al., 2005
Fernandez, X.; Lizzani-Cuvelier, L.; Loiseau, A.-M.; Perichet, C.; Delbecque, C.; Arnaudo, J.-F., Chemical composition of the essential oils from Turkish and Honduras Styrax, Flavour Fragr. J., 2005, 20, 1, 70-73, https://doi.org/10.1002/ffj.1370 . [all data]

Park, Lee, et al., 2004
Park, B.-S.; Lee, K.-G.; Takeoka, G.R., Comparison of three sample preparation methods on the recovery of volatiles from taheebo (Tabebuia impetiginosa Martius ex DC), Flavour Fragr. J., 2004, 19, 4, 287-292, https://doi.org/10.1002/ffj.1345 . [all data]

Wang and Guo-Y. -L., 2004
Wang, H.-Y.; Guo-Y. -L., Rapid analysis of the volatile compounds in the rhizomes of Rhodiola sachalinensis and Rhodiola sacra by static headspace-gas chromatography-tandem mass spectrometry, Anal. Letters, 2004, 37, 10, 2151-2161, https://doi.org/10.1081/AL-200026690 . [all data]

Egolf and Jurs, 1993
Egolf, L.M.; Jurs, P.C., Quantitative structure-retention and structure-odor intensity relationships for a diverse group of odor-active compounds, Anal. Chem., 1993, 65, 21, 3119-3126, https://doi.org/10.1021/ac00069a027 . [all data]

Okumura, 1991
Okumura, T., retention indices of environmental chemicals on methyl silicone capillary column, Journal of Environmental Chemistry (Japan), 1991, 1, 2, 333-358, https://doi.org/10.5985/jec.1.333 . [all data]


Notes

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