Benzeneacetic acid, ethyl ester

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-5RTX-5RTX-5HP-5MS
Column length (m) 30.10.30.30.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.180.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Tstart (C) 50.40.40.40.60.
Tend (C) 250.275.300.300.250.
Heat rate (K/min) 4.50.5.5.4.
Initial hold (min) 4.0.52.2.2.
Final hold (min) 10.0.510.10.20.
I 1247.1251.1224.91223.91244.
ReferenceQuijano, Salamanca, et al., 2007Setkova, Risticevic, et al., 2007Ádámová, Orinák, et al., 2005Ádámová, Orinák, et al., 2005Pino, Mesa, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-1DB-1DB-1
Column length (m) 30.30.30.30.30.
Carrier gas He    
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25    
Tstart (C) 60.50.50.50.50.
Tend (C) 250.300.300.300.300.
Heat rate (K/min) 4.2.2.2.2.
Initial hold (min) 2.    
Final hold (min) 20.    
I 1249.1210.81211.71210.81213.0
ReferencePino, Marbot, et al., 2004Chang, Sheng, et al., 1989Chang, Sheng, et al., 1989Chang, Sheng, et al., 1989Chang, Sheng, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase BP-1OV-1
Column length (m) 12.25.
Carrier gas H2He
Substrate   
Column diameter (mm)  0.32
Phase thickness (μm)   
Tstart (C) 40.40.
Tend (C) 240.280.
Heat rate (K/min) 4.8.
Initial hold (min) 2. 
Final hold (min) 75.10.
I 1209.1224.
ReferenceTan, Wilkins, et al., 1989Tan, Holland, et al., 1988
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Quijano, Salamanca, et al., 2007
Quijano, C.E.; Salamanca, G.; Pino, J.A., Aroma volatile constituents of Colombian varieties of mango (Mangifera indica L.), Flavour Fragr. J., 2007, 22, 5, 401-406, https://doi.org/10.1002/ffj.1812 . [all data]

Setkova, Risticevic, et al., 2007
Setkova, L.; Risticevic, S.; Pawliszyn, J., Rapid headspace solid-phase microextraction-gas chromatographic-time-of-flight mass spectrometric method for qualitative profiling of ice wine volatile fraction I. Method development and optimization, J. Chromatogr. A, 2007, 1147, 2, 213-223, https://doi.org/10.1016/j.chroma.2007.02.058 . [all data]

Ádámová, Orinák, et al., 2005
Ádámová, M.; Orinák, A.; Halás, L., Retention indices as identification tool in pyrolysis-capillary gas chromatography, J. Chromatogr. A, 2005, 1087, 1-2, 131-141, https://doi.org/10.1016/j.chroma.2005.01.003 . [all data]

Pino, Mesa, et al., 2005
Pino, J.A.; Mesa, J.; Muñoz, Y.; Martí, M.P.; Marbot, R., Volatile components from mango (Mangifera indica L.) cultivars, J. Agric. Food Chem., 2005, 53, 6, 2213-2223, https://doi.org/10.1021/jf0402633 . [all data]

Pino, Marbot, et al., 2004
Pino, J.A.; Marbot, R.; Rosado, A.; Vázquez, C., Volatile constituents of Malay rose apple [Syzygium malaccense (L.) Merr. Perry], Flavour Fragr. J., 2004, 19, 1, 32-35, https://doi.org/10.1002/ffj.1269 . [all data]

Chang, Sheng, et al., 1989
Chang, L.P.; Sheng, L.S.; Yang, M.Z.; An, D.K., Retention index of essential oil in temperature-programmed capillary column gas chromatography, Acta Pharm. Sin., 1989, 24, 11, 847-852. [all data]

Tan, Wilkins, et al., 1989
Tan, S.T.; Wilkins, A.L.; Holland, P.T.; McGhie, T.K., Extractives from New Zealand unifloral honeys. 2. Degraded carotenoids and other substances from heather honey, J. Agric. Food Chem., 1989, 37, 5, 1217-1221, https://doi.org/10.1021/jf00089a004 . [all data]

Tan, Holland, et al., 1988
Tan, S.-T.; Holland, P.T.; Wilkins, A.L.; Molan, P.C., Extractives from New Zealand honeys. 1. White clovers, manuka, and kanuka unifloral honeys, J. Agric. Food Chem., 1988, 36, 3, 453-460, https://doi.org/10.1021/jf00081a012 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References