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Ethylbenzene

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Kovats' RI, polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase Carbowax 20MCarbowax 20MSupelcowax-10PEG-20MCarbowax 20M
Column length (m) 15.15.60.30.2.
Carrier gas HeHeN2N2He
Substrate     A silanized white support
Column diameter (mm) 0.50.50.750.3 
Phase thickness (mum)      
Temperature (C) 150.150.60.70.110.
I 1100.1105.1138.1131.91158.9
ReferenceEgazaryants and Maximov, 1998Egazaryants and Maximov, 1998Castello, Vezzani, et al., 1991Tóth, 1983Vernon and Suratman, 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 2.2.2.2. 
Carrier gas HeHeHeN2 
Substrate A silanized white supportA silanized white supportA silanized white supportKieselgur (60-100 mesh)Chromosorb W, AW-DMCS
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 120.130.140.75.150.
I 1164.31169.81175.21136.1160.9
ReferenceVernon and Suratman, 1983Vernon and Suratman, 1983Vernon and Suratman, 1983Goebel, 1982Ellis and Still, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedCapillaryCapillaryPacked
Active phase Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20MPEG-2000
Column length (m)   100.100.3.
Carrier gas   N2 He
Substrate Chromosorb GChromosorb G  Celite 545 (44-60 mesh)
Column diameter (mm)   0.230.2 
Phase thickness (mum)      
Temperature (C) 115.115.100.90.152.
I 1158.41159.41127.11111.11178.
ReferenceEllis and Still, 1979Ellis and Still, 1979Engewald and Wennrich, 1976Döring, Estel, et al., 1974Anderson, Jurel, et al., 1973
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPacked
Active phase Polyethylene Glycol 4000Polyethylene Glycol 4000Polyethylene Glycol 4000Polyethylene Glycol 4000
Column length (m) 6.6.6.6.
Carrier gas     
Substrate Chromosorb PChromosorb PChromosorb PChromosorb P
Column diameter (mm)     
Phase thickness (mum)     
Temperature (C) 100.120.140.80.
I 1154.1162.1169.1147.
ReferenceBonastre and Grenier, 1967Bonastre and Grenier, 1967Bonastre and Grenier, 1967Bonastre and Grenier, 1967
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Egazaryants and Maximov, 1998
Egazaryants, S.V.; Maximov, A.L., Analysis of Gasoline Fractions by Capillary GC in 20th International Symposium on Capillary Chromatography, 1998, 1-6. [all data]

Castello, Vezzani, et al., 1991
Castello, G.; Vezzani, S.; Gerbino, T., Gas chromatographic separation and automatic identification of complex mixtures of organic solvents in indrustrial wates, J. Chromatogr., 1991, 585, 2, 273-280, https://doi.org/10.1016/0021-9673(91)85088-W . [all data]

Tóth, 1983
Tóth, T., Use of capillary gas chromatography in collecting retention and chemical information for the analysis of complex petrochemical mixtures, J. Chromatogr., 1983, 279, 157-165, https://doi.org/10.1016/S0021-9673(01)93614-3 . [all data]

Vernon and Suratman, 1983
Vernon, F.; Suratman, J.B., The retention index system applied to alkylbenzenes and monosubstituted derivatives, Chromatographia, 1983, 17, 11, 600-604, https://doi.org/10.1007/BF02261943 . [all data]

Goebel, 1982
Goebel, K.-J., Gaschromatographische Identifizierung Niedrig Siedender Substanzen Mittels Retentionsindices und Rechnerhilfe, J. Chromatogr., 1982, 235, 1, 119-127, https://doi.org/10.1016/S0021-9673(00)95793-5 . [all data]

Ellis and Still, 1979
Ellis, T.S.; Still, R.H., Thermal degradation of polymers. XXI. Vacuum pyrolysis of poly(m-N,N-dimethylaminostyrene); the products volatile at pyrolysis temperature, liquid at room temperature, J. Appl. Polym. Sci., 1979, 23, 10, 2837-2854, https://doi.org/10.1002/app.1979.070231002 . [all data]

Engewald and Wennrich, 1976
Engewald, W.; Wennrich, L., Molekülstruktur und Retentionsverhalten. VIII. Zum Retentionsverhalten höherer Alkylbenzole bei der Gas-Verteilungs-Chromatographie, Chromatographia, 1976, 9, 11, 540-547, https://doi.org/10.1007/BF02275960 . [all data]

Döring, Estel, et al., 1974
Döring, C.E.; Estel, D.; Fischer, R., Kapillar-gaschromatographische Charakterisierung von C10-bis C12-Aromaten, J. Prakt. Chem., 1974, 316, 1, 1-12, https://doi.org/10.1002/prac.19743160102 . [all data]

Anderson, Jurel, et al., 1973
Anderson, A.; Jurel, S.; Shymanska, M.; Golender, L., Gas-liquid chromatography of some aliphatic and heterocyclic mono- and pollyfunctional amines. VII. Retention indices of amines in some polar and unpolar stationary phases, Latv. PSR Zinat. Akad. Vestis Kim. Ser., 1973, 1, 51-63. [all data]

Bonastre and Grenier, 1967
Bonastre, J.; Grenier, P., Contribution à l'étude de la polarité des phases stationnaires en chromatographie gas-liquide. I. Calcul des coefficients d'activité relatifs et des indices de rétention de quelques hydrocarbures aromatiques, Bull. Soc. Chim. Fr., 1967, 4, 1395-1405. [all data]


Notes

Go To: Top, Kovats' RI, polar column, isothermal, References