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Ethylbenzene

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Kovats' RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5SPB-1SE-54
Column length (m) 60.60.30.50.30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.200.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 30.30.50.35.0.
Tend (C) 220.220.300.200.250.
Heat rate (K/min) 2.2.6.3.12.
Initial hold (min) 4.4.2.5.12.
Final hold (min)    20. 
I 844.848.864.1844.853.
ReferenceTakeoka, Perrino, et al., 1996Takeoka, Perrino, et al., 1996Wang, Fingas, et al., 1994Wong and Tie, 1993Rembold, Wallner, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101SE-30SE-30OV-101
Column length (m) 50.110.50.50.70.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.230.250.50.50.28
Phase thickness (mum)  0.20   
Tstart (C) 80.35.40.40.80.
Tend (C) 200.200.170.170.200.
Heat rate (K/min) 2.1.3.3.2.
Initial hold (min)   3.3. 
Final hold (min)      
I 858.843.850.851.855.
ReferenceOhnishi and Shibamoto, 1984Hayes and Pitzer, 1982Greenberg, 1981Greenberg, 1981Yamaguchi and Shibamoto, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-101Apiezon L
Column length (m) 70.50.
Carrier gas N2N2
Substrate   
Column diameter (mm) 0.280.25
Phase thickness (mum)   
Tstart (C) 80.60.
Tend (C) 200. 
Heat rate (K/min) 2.1.
Initial hold (min)   
Final hold (min)   
I 857.868.
ReferenceYamaguchi and Shibamoto, 1981Louis, 1971
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Takeoka, Perrino, et al., 1996
Takeoka, G.; Perrino, C., Jr.; Buttery, R., Volatile constituents of used frying oils, J. Agric. Food Chem., 1996, 44, 3, 654-660, https://doi.org/10.1021/jf950430m . [all data]

Wang, Fingas, et al., 1994
Wang, Z.; Fingas, M.; Li, K., Fractionation of a light crude oil and identification and quantitation of aliphatic, aromatic, and biomarker comopunds by GC-FID and GC-MS, Part II, J. Chromatogr. Sci., 1994, 32, 9, 367-382, https://doi.org/10.1093/chromsci/32.9.367 . [all data]

Wong and Tie, 1993
Wong, K.C.; Tie, D.Y., The Essential Oil of the Leaves of Murraya koenigii Spreng., J. Essent. Oil Res., 1993, 5, 4, 371-374, https://doi.org/10.1080/10412905.1993.9698245 . [all data]

Rembold, Wallner, et al., 1989
Rembold, H.; Wallner, P.; Nitz, S.; Kollmannsberger, H.; Drawert, F., Volatile components of chickpea (Cicer arietinum L.) seed, J. Agric. Food Chem., 1989, 37, 3, 659-662, https://doi.org/10.1021/jf00087a018 . [all data]

Ohnishi and Shibamoto, 1984
Ohnishi, S.; Shibamoto, T., Volatile compounds from heated beef fat and beef fat with glycine, J. Agric. Food Chem., 1984, 32, 5, 987-992, https://doi.org/10.1021/jf00125a008 . [all data]

Hayes and Pitzer, 1982
Hayes, P.C., Jr.; Pitzer, E.W., Characterizing petroleum- and shale-derived jet fuel distillates via temperature-programmed Kováts indices, J. Chromatogr., 1982, 253, 179-198, https://doi.org/10.1016/S0021-9673(01)88376-X . [all data]

Greenberg, 1981
Greenberg, M.J., Characterization of meat and bone meal flavor volatiles, J. Agric. Food Chem., 1981, 29, 6, 1276-1280, https://doi.org/10.1021/jf00108a043 . [all data]

Yamaguchi and Shibamoto, 1981
Yamaguchi, K.; Shibamoto, T., Volatile constituents of green tea, Gyokuro (Camellia sinensis L. var Yabukita), J. Agric. Food Chem., 1981, 29, 2, 366-370, https://doi.org/10.1021/jf00104a035 . [all data]

Louis, 1971
Louis, R., Kovats-index-tafeln zur gaschromatographischen analyse von kohlenwasserstoffgemischen, Erdoel Kohle Erdgas Petrochem., 1971, 24, 2, 88-94. [all data]


Notes

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