Alprenolol, TBDMS derivative
- Formula: C21H37NO2Si
- Molecular weight: 363.6095
- IUPAC Standard InChI: InChI=1S/C21H37NO2Si/c1-9-12-18-13-10-11-14-20(18)23-16-19(15-22-17(2)3)24-25(7,8)21(4,5)6/h9-11,13-14,17,19,22H,1,12,15-16H2,2-8H3
- IUPAC Standard InChIKey: VRQHRSXIGWWRJE-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Alprenolol, tert-butyldimethylsilyl ether; Alprenolol, TBDMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5MS | 2069.7 | Paik, Nguyen, et al., 2006 | 15. m/0.25 mm/0.25 μm, He, 100. C @ 1. min, 10. K/min, 290. C @ 10. min |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 2084.1 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Paik, Nguyen, et al., 2006
Paik, M.-J.; Nguyen, D.T.; Kim, K.-R.,
GC and MS Properties of b-Blockers as tert-Butyldimethylsilyl Derivatives and as Ethoxycarbonyl/Trimethylsilyl Derivatives,
Chromatographia, 2006, 64, 11-12, 673-679, https://doi.org/10.1365/s10337-006-0095-4
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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