1,2,4,5-tetraoxacyclohexane, 3,3,6,6-tetraethyl
- Formula: C10H20O4
- Molecular weight: 204.2634
- IUPAC Standard InChI: InChI=1S/C10H20O4/c1-5-9(6-2)11-13-10(7-3,8-4)14-12-9/h5-8H2,1-4H3
- IUPAC Standard InChIKey: VGCWOVJYNWNYIM-UHFFFAOYSA-N
- Chemical structure:
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-5 | DB-5 | DB-5 | RTX-5 MS | RTX-5 MS |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | N2 | N2 | N2 | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 60. | 60. | 60. | 60. | 60. |
| Tend (C) | 300. | 300. | 300. | 300. | 300. |
| Heat rate (K/min) | 10. | 20. | 5. | 10. | 20. |
| Initial hold (min) | 5. | 5. | 5. | 5. | 5. |
| Final hold (min) | |||||
| I | 1227.3 | 1237.3 | 1229.6 | 1240.1 | 1245.9 |
| Reference | Barreto, Cañizo, et al., 2006 | Barreto, Cañizo, et al., 2006 | Barreto, Cañizo, et al., 2006 | Barreto, Cañizo, et al., 2006 | Barreto, Cañizo, et al., 2006 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | RTX-5 MS | RTX-5 MS |
| Column length (m) | 30. | 30. |
| Carrier gas | He | He |
| Substrate | ||
| Column diameter (mm) | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 |
| Tstart (C) | 60. | 60. |
| Tend (C) | 300. | 300. |
| Heat rate (K/min) | 5. | 10. |
| Initial hold (min) | 5. | |
| Final hold (min) | ||
| I | 1238.2 | 1238.6 |
| Reference | Barreto, Cañizo, et al., 2006 | Barreto, Cañizo, et al., 2006 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Barreto, Cañizo, et al., 2006
Barreto, G.P.; Cañizo, A.I.; Eyler, G.N.,
Use of Retention Data as the First Step in the Identification of Cyclic Organic Peroxides in Temperature-Programmed Gas Chromatography,
Chromatographia, 2006, 63, 5-6, 261-266, https://doi.org/10.1365/s10337-006-0716-y
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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