Glycine-threonine-phenylalanine, N(α,ε)-trifluoroacetyl-N-O-permethyl derivative
- Formula: C22H30F3N3O6
- Molecular weight: 489.4853
- IUPAC Standard InChI: InChI=1S/C22H30F3N3O6/c1-14(33-5)18(28(4)17(29)13-26(2)21(32)22(23,24)25)19(30)27(3)16(20(31)34-6)12-15-10-8-7-9-11-15/h7-11,14,16,18H,12-13H2,1-6H3
- IUPAC Standard InChIKey: YNJPSXZBYFXIQK-UHFFFAOYSA-N
- Chemical structure:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | CP Sil 5 CB | 2582. | Rose, Bairoch, et al., 1983 | 5. m/0.34 mm/0.4 μm, He, 80. C @ 1. min, 4. K/min; Tend: 320. C |
| Capillary | SE-54 | 2665. | Rose, Bairoch, et al., 1983 | 5. m/0.34 mm/0.4 μm, He, 80. C @ 1. min, 4. K/min; Tend: 320. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Rose, Bairoch, et al., 1983
Rose, K.; Bairoch, A.; Offord, R.E.,
Amino acid sequence determination by gas chromatography-mass spectrometry of permethylated peptides. The application of capillary columns,
J. Chromatogr., 1983, 268, 197-206, https://doi.org/10.1016/S0021-9673(01)95406-8
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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