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Germacrone


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryBP-11677.Srivastava, Srivastava, et al., 200630. m/0.32 mm/0.25 «mu»m, N2, 5. K/min, 220. C @ 3. min; Tstart: 60. C
CapillaryDB-51693.Sylvestre, Pichette, et al., 200630. m/0.25 mm/0.25 «mu»m, 40. C @ 2. min, 2. K/min, 210. C @ 33. min
CapillaryBP-11669.Raina, Srivastava, et al., 200225. m/0.55 mm/0.25 «mu»m, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryDB-51691.Loayza, Abujder, et al., 199540. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m
CapillaryDB-51696.Loayza, Abujder, et al., 199540. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m
CapillaryMethyl Silicone1691.3Rao, Rajanikanth, et al., 19894. K/min, 250. C @ 15. min; Column length: 12. m; Column diameter: 0.5 mm; Tstart: 70. C

Kovats' RI, polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillarySupelcowax-102217.Sylvestre, Pichette, et al., 200630. m/0.25 mm/0.25 «mu»m, 40. C @ 2. min, 2. K/min, 210. C @ 33. min
CapillarySupelcowax-102209.Loayza, Abujder, et al., 199540. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m
CapillarySupelcowax-102212.Loayza, Abujder, et al., 199540. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryMethyl Silicone1689.Melo, Corrêa, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 15. min; Tstart: 80. C
CapillaryHP-51693.Bertoli, Pistelli, et al., 200430. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
CapillaryHP-5MS1707.9Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)

Normal alkane RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryDB-51694.Rodriques, Amorim, et al., 201330. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5 MS1705.Radulovic, Blagojevic, et al., 201030. m/0.25 mm/0.25 «mu»m, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C
CapillaryUltra 21733.Byun and Shin, 200850. m/0.20 mm/0.11 «mu»m, Helium, 60. C @ 5. min, 2. K/min, 230. C @ 30. min
CapillaryElite-11690.Raj, Baby, et al., 200830. m/0.32 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryCP-Sil 5 CB1705.Olawore, Usman, et al., 200625. m/0.25 mm/0.15 «mu»m, Hydrogen, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryCP Sil 5 CB1675.Tesso, König, et al., 2006H2, 3. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 230. C
CapillaryDB-5MS1658.Marongiu, Piras, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 60. C @ 30. min, 3. K/min; Tend: 280. C
CapillaryHP-51688.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 «mu»m, 40. C @ 15. min, 5. K/min; Tend: 250. C
CapillaryHP-51690.Velickovic, Ristic, et al., 200325. m/0.32 mm/0.53 «mu»m, Helium, 4. K/min; Tstart: 40. C; Tend: 280. C
CapillaryHP-51694.Velickovic, Ristic, et al., 200325. m/0.32 mm/0.53 «mu»m, Helium, 4. K/min; Tstart: 40. C; Tend: 280. C

Normal alkane RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
CapillaryDB-51693.Rodriques, Amorim, et al., 201330. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryElite-11694.Raj, Baby, et al., 200830. m/0.32 mm/0.25 «mu»m, Helium; Program: not specified
CapillarySE-301694.Vinogradov, 2004Program: not specified
CapillaryCP Sil 5 CB1687.Phan, Van, et al., 1998N2; Column length: 25. m; Program: not specified
CapillaryPolydimethyl siloxanes1694.Zenkevich, 1997Program: not specified
CapillaryDB-11644.de Morais, Craveiro, et al., 1996Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: 35 0C 4 0C/min -> 180 0C 10 0C/min -> 250 0C

Normal alkane RI, polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryDB-Wax2223.Molleken U., Sinnwell V., et al., 199830. m/0.25 mm/0.25 «mu»m, N2, 3. K/min; Tstart: 45. C; Tend: 220. C
CapillaryDB-Wax2254.Mölleken, Sinnwell, et al., 199830. m/0.25 mm/0.25 «mu»m, N2, 3. K/min; Tstart: 45. C; Tend: 220. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Srivastava, Srivastava, et al., 2006
Srivastava, A.K.; Srivastava, S.K.; Syamsundar, K.V., Volatile composition of Curcuma angustifolia Roxb. rhizome from central and southern India, Flavour Fragr. J., 2006, 21, 3, 423-426. [doi:10.1002/ffj.1680] [all data]

Sylvestre, Pichette, et al., 2006
Sylvestre, M.; Pichette, A.; Longtin, A.; Nagau, F.; Legault, J., Essential oil analysis and anticancer activity of leaf essential oil of Croton flavens L. from Guadeloupe, J. Ethnopharmacol., 2006, 103, 1, 99-102. [doi:10.1016/j.jep.2005.07.011] [all data]

Raina, Srivastava, et al., 2002
Raina, V.K.; Srivastava, S.K.; Jain, N.; Ahmad, A.; Syamasundar, K.V.; Aggarwal, K.K., Essential oil composition of Curcuma longa L. cv. Roma from the plains of northern India, Flavour Fragr. J., 2002, 17, 2, 99-102. [doi:10.1002/ffj.1053] [all data]

Loayza, Abujder, et al., 1995
Loayza, I.; Abujder, D.; Aranda, R.; Jakupovic, J.; Collin, G.; Deslauriers, H.; Jean, F.-I., Essential oils of Baccharis salicifolia, B. latifolia and B. dracunculifolia, Phytochemistry, 1995, 38, 2, 381-389. [doi:10.1016/0031-9422(94)00628-7] [all data]

Rao, Rajanikanth, et al., 1989
Rao, A.S.; Rajanikanth, B.; Seshadri, R., Volatile aroma components of Curcuma amada Roxb., J. Agric. Food Chem., 1989, 37, 3, 740-743. [doi:10.1021/jf00087a036] [all data]

Melo, Corrêa, et al., 2007
Melo, R.M.; Corrêa, V.F.S.; Amorim, A.C.L.; Miranda, A.L.P.; Rezende, C.M., Identification of Impact Aroma Compounds in Eugenia uniflora L. (Brazilian Pitanga) Leaf Essential Oil, J. Braz. Chem. Soc., 2007, 18, 1, 179-183. [doi:10.1590/S0103-50532007000100020] [all data]

Bertoli, Pistelli, et al., 2004
Bertoli, A.; Pistelli, L.; Morelli, I.; Fraternale, D.; Giamperi, L.; Ricci, D., Volatile constituents of different parts (roots, stems and leaves) of Smyrnium olusatrum L., Flavour Fragr. J., 2004, 19, 6, 522-525. [doi:10.1002/ffj.1382] [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Rodriques, Amorim, et al., 2013
Rodriques, K.A. da.F.; Amorim, L.V.; de Oliveira, J.M.G.; Dias, C.N.; Moraes, D.F.C.; Andrade, E.H. deA.; Maia, J.G.S.; Carneiro, S.M.P.; Carvalho, F.A. deA., Eugenia uniflora L. essential oil as a potential anti-Leishmania agent: effect on Leishmania amazonensis and possible mechanism of action, Evidence-Based Complementary and Alternative Medicine, 2013, 2013, 1-10. [doi:10.1155/2013/279726] [all data]

Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185. [doi:10.3390/molecules15096168] [all data]

Byun and Shin, 2008
Byun, Y.; Shin, S., Analysis of compounds and activity of essential oil from Chrysanthemum zawadskii var. latilobum and C. indicum agaunst antibiotic-resistant pathogenic bacteria, Nat. Prod. Sci., 2008, 14, 2, 138-142. [all data]

Raj, Baby, et al., 2008
Raj, G.; Baby, S.; Dan, M.; Thaha, A.R.M.; Sethuraman, M.G.; George, V., Volatile constituents from the rhisomes of Curcuma haritha Mangaly and Sabu from Sauthern India, Flavour Fragr. J., 2008, 23, 5, 348-352. [doi:10.1002/ffj.1891] [all data]

Olawore, Usman, et al., 2006
Olawore, N.O.; Usman, L.A.; Ogunwande, I.A.; Adeleke, K.A., Constituents of rhizome essential oils of two types of Cyperus articulatus L. grown in Nigeria, J. Essent Oil Res., 2006, 18, 6, 604-606. [doi:10.1080/10412905.2006.9699179] [all data]

Tesso, König, et al., 2006
Tesso, H.; König, W.A.; Son, P.T.; Giang, P.M., Composition of the essential oil of flowers of Chloranthus spicatus (Thunb.) Makino, Flavour Fragr. J., 2006, 21, 4, 592-597. [doi:10.1002/ffj.1528] [all data]

Marongiu, Piras, et al., 2005
Marongiu, B.; Piras, A.; Porcedda, S.; Scorciapino, A., Chemical composition of the essential oil and supercritical CO2 extract of Commiphora myrrha (Nees) Engl. and of Acorus calamus L., J. Agric. Food Chem., 2005, 53, 20, 7939-7943. [doi:10.1021/jf051100x] [all data]

Stashenko, Jaramillo, et al., 2003
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Comparación de la composición química y de la actividad antioxidante in vitro de los metabolitos secundarios volátiles de plantas de la familia verbenaceae, Rev. Acad. Colomb. Cienc. Exactas Fis. Nat., 2003, 27, 105, 579-597. [all data]

Velickovic, Ristic, et al., 2003
Velickovic, A.S.; Ristic, M.S.; Velickovic, D.T.; Ilic, S.; Mitic, N.D., The possibilities of the application of some species of sage (Salvia L.) as auxiliaries in the treatment of some diseases, J. Serb. Chem. Soc., 2003, 68, 6, 435-445. [doi:10.2298/JSC0306435V] [all data]

Vinogradov, 2004
Vinogradov, B.A., Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]

Phan, Van, et al., 1998
Phan, M.G.; Van, N.H.; Phan, T.S., Sesquiterpenoids fron the rhizomes of Curcuma aff. aeruginosa Roxb. of Vietnam, Tap chi Hoa hoc, 1998, 36, 3, 67-72. [all data]

Zenkevich, 1997
Zenkevich, I.G., Analytical Parameters of Components of Essential Oils for their Chromatographic and Chromato-Spectral Identificaiton. Oxsigenated derivatives of Mono- and Sesquiterpene Hydrocarbons, Rastit, Resursy (Rus.), 1997, 33, 1, 16-28. [all data]

de Morais, Craveiro, et al., 1996
de Morais, S.M.; Craveiro, A.A.; Machado, M.I.L.M.; Alencar, J.W.; Matos, J.A., Volatile constituents of Eugenia unifluora leaf oil from Notheastern Brazil, J. Ess. Oil Res., 1996, 8, 4, 449-451. [doi:10.1080/10412905.1996.9700664] [all data]

Molleken U., Sinnwell V., et al., 1998
Molleken U.; Sinnwell V.; Kubeczka K.H., TThe essential oil composition of fruits from Smyrnium perfoliatum, Phytochemistry, 1998, 47, 6, 1079-1083. [doi:10.1016/S0031-9422(98)80076-9] [all data]

Mölleken, Sinnwell, et al., 1998
Mölleken, U.; Sinnwell, V.; Kubeczka, K.-H., Essential oil composition of Smyrnium olusatrum, Phytochemistry, 1998, 49, 6, 1709-1714. [doi:10.1016/S0031-9422(98)00195-2] [all data]


Notes

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