2-Furancarboxaldehyde, 5-methyl-

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Normal alkane RI, polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxHP-InnowaxSupelko CO Wax
Column length (m) 60.30.30.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.200.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Program 40 0C (3 min) 2 0C/min -> 150 0C 4 0C/min -> 220 0C (20 min) 5 0C/min -> 230 0Cnot specifiednot specified40 0C (2 min) 3 0C/min -> 150 0C 5 0C/min -> 220 0C (5 min)40 0C (5 min) 4 0C/min -> 75 0C 5 0C/min -> 250 0C (10 min)
I 1569.1570.1600.1591.1578.
ReferenceGyawali and Kim, 2012Welke, Manfroi, et al., 2012Welke, Manfroi, et al., 2012Xiao, Dai, et al., 2011Vekiari, Orepoulou, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelko CO WaxStabilwaxDB-FFAPDB-FFAPSupelcowax-10
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified35 0C 3 0C/min -> 100 0C 5 0C/min -> 240 0C (10 min)50 0C 2 0C/min -> 100 0C (5 min) 5 0C/min -> 250 0Cnot specified45 0C 3 0C/min -> 230 0C (10 min) 10 0C/min -> 270 0C (21 min)
I 1578.1567.1544.1560.1551.
ReferenceVekiari, Orepoulou, et al., 2010Chinnici, Guerrero, et al., 2009Mebazaa, Mahmoudi, et al., 2009Mebazaa, Mahmoudi, et al., 2009de Simon, Estruelas, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax 10DB-WaxSupelcowax-10DB-Wax
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeliumHeliumHeHydrogen
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified45 0C (15 min) 3 0C/min -> 75 0C 5 0C/min -> 180 0C (10 min)50 0C 20 0C/min -> 80 0C 3 0C/min -> 230 0C40C(10min) => 2C/min => 200C(1min) => 2C/min => 250C (10min)44 0C 3 0C/min -> 170 0C 8 0C/min -> 250 0C
I 1566.1588.1556.1572.1566.
ReferenceZhao, Xu, et al., 2009Soria, Martinez-Castro, et al., 2008Tao, Wenlai, et al., 2008Bosch-Fuste, Riu-Aumatell, et al., 2007Gonzalez-Rios, Suarez-Quiroz, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP-InnowaxBP-20BP-20DB-Wax
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified30 0C (5 min) 5 0C/min -> 100 0C (5 min) 1 0C/min -> 130 0C 10 0C/min -> 195 0C (45 min)50C(1min) => 2.5C/min => 100C => 2C/min => 180C => 15C/min => 220C50C(1min) => 2.5C/min => 100C => 2C/min => 180C => 15C/min => 220C50 0C (2 min) 6 0C/min -> 150 0C 8 0C/min -> 230 0C (15 min)
I 1563.1586.1569.1569.1561.
ReferenceGonzalez-Rios, Suarez-Quiroz, et al., 2007Narain, Galvao, et al., 2007Pontes, Marques, et al., 2007Pontes, Marques, et al., 2007Tian, Zhang, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxHP-InnowaxHP-InnowaxInnowax FSCDB-Wax
Column length (m) 60.60.30.60.60.
Carrier gas HeliumHeliumHeHeHelium
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.250.250.50.250.25
Program 40 0C (5 min) 4 0C/min -> 60 0C (5 min) 8 0C/min -> 250 0C (3 min)not specified30C(2min) => 4C/min => 130C => 8C/min => 250C(5min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (3 min) 2 0C/min -> 150 0C 4 0C/min -> 200 0C
I 1588.1570.1610.1585.1552.
ReferenceViegas and Bassoli, 2007Viegas and Bassoli, 2007Weldegergis B.T., Tredoux A.G.J., et al., 2007Baser, Özek, et al., 2004Kim. J.H., Ahn, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxCarbowax 20MHP-InnowaxSupelcowax-10Nukol
Column length (m) 60. 30. 25.
Carrier gas He He N2
Substrate      
Column diameter (mm) 0.25 0.32 0.25
Phase thickness (μm) 0.25 0.5  
Program 50C(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified50C(4min) => 10C/min => 230C(10min) => 10C/min => 250Cnot specified45C(5min) => 20C/min => 100C(1min) => 3C/min => 190C(40min)
I 1586.1576.1586.1523.1570.
ReferenceSelli, Kürkçüoglu, et al., 2004Vinogradov, 2004Piasenzotto, Gracco, et al., 2003Jung, Kim, et al., 2001López and Dufour, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MPEGDB-WaxSupelcowax-10Supelcowax-10
Column length (m) 50.40.60.30.30.
Carrier gas N2HydrogenN2HeHe
Substrate      
Column diameter (mm) 0.20.182 0.320.32
Phase thickness (μm) 0.20.300.250.25 
Program 60C => 2C/min => 150C => 4C/min => 220C35 0C (5 min) 5 0C/min -> 100 0C 3 0C/min -> 200 0C (1 min) 20 0C/min -> 240 0C (2 min)not specified50C(2min) => 7C/min => 140C => 17.5C/min => 230C35C => 40C/min => 60C(2min) => 4C/min => 240C
I 1577.1590.1586.1563.1555.
ReferenceTeai, Claude-Lafontaine, et al., 2001Vas, Gal, et al., 1998Weyerstahl, Marschall, et al., 1998Chang, Seitz, et al., 1995Schieberle and Grosch, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase DB-WaxCarbowax 400, Carbowax 20M, Carbowax 1540, Carbowax 4000, Superox 06, PEG 20M, etc.
Column length (m)  50.
Carrier gas  Hydrogen
Substrate   
Column diameter (mm)  0.32
Phase thickness (μm)   
Program not specifiednot specified
I 1562.1551.
ReferencePeng, Yang, et al., 1991Waggott and Davies, 1984
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Gyawali and Kim, 2012
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Welke, Manfroi, et al., 2012
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Vekiari, Orepoulou, et al., 2010
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Mebazaa, Mahmoudi, et al., 2009
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de Simon, Estruelas, et al., 2009
de Simon, B.F.; Estruelas, E.; Munoz, A.M.; Cadahia, E.; Sanz, M., Volatile compounds in acacia, chestnut, cherry, ash, and oak woods, with a view to their use in cooperage, J. Agric. Food Chem., 2009, 57, 8, 3217-3227, https://doi.org/10.1021/jf803463h . [all data]

Zhao, Xu, et al., 2009
Zhao, Y.; Xu, Y.; Li, J.; Fan, W.; Jiang, W., Profile of volatile compounds in 11 brandies by headspace solid-phase microextraction followed by gas chromatography-mass spectrometry, J. Food. Sci., 2009, 74, 2, c90-c99, https://doi.org/10.1111/j.1750-3841.2008.01029.x . [all data]

Soria, Martinez-Castro, et al., 2008
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Tao, Wenlai, et al., 2008
Tao, L.; Wenlai, F.; Yan, X., Characterization of volatile and semi-volatile compounds in Chinese rica wines by headspace solid phase microextraction followed by gas chromatography - mass spectrometry, J. Inst. Brew., 2008, 114, 2, 172-179, https://doi.org/10.1002/j.2050-0416.2008.tb00323.x . [all data]

Bosch-Fuste, Riu-Aumatell, et al., 2007
Bosch-Fuste, J.; Riu-Aumatell, M.; Guadayol, J.M.; Caixach, J.; Lopez-Tamames, E.; Buxaderas, S., Volatile profiles of sparkling wines obtained by three extraction methods and gas chromatography-mass spectrometry (GC-MS) analysis, Food Chem., 2007, 105, 1, 428-435, https://doi.org/10.1016/j.foodchem.2006.12.053 . [all data]

Gonzalez-Rios, Suarez-Quiroz, et al., 2007
Gonzalez-Rios, O.; Suarez-Quiroz, M.L.; Boulanger, R.; Barel, M.; Guyot, B.; Guiraud, J.-P.; Schorr-Galindo, S., Impact of ecological post-harvest processing of coffee aroma: II Roasted coffee., J. Food Composition Analysis, 2007, 20, 3-4, 297-307, https://doi.org/10.1016/j.jfca.2006.12.004 . [all data]

Narain, Galvao, et al., 2007
Narain, N.; Galvao, M. deS.; Ferreira, D.DaS.; Navarro, D.M.A.F., Flavor biogeneration in Mangaba (Hancornia speciosa Gomes) fruit, BioEng. Campinas, 2007, 1, 1, 25-31. [all data]

Pontes, Marques, et al., 2007
Pontes, M.; Marques, J.C.; Camara, J.S., Screening of volatile composition from Portuguese multifloral honeys using headspace solid-phase microextraction-gas chromatography-quadrupole mass spectrometry, Talanta, 2007, 74, 1, 91-103, https://doi.org/10.1016/j.talanta.2007.05.037 . [all data]

Tian, Zhang, et al., 2007
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Viegas and Bassoli, 2007
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Weldegergis B.T., Tredoux A.G.J., et al., 2007
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Notes

Go To: Top, Normal alkane RI, polar column, custom temperature program, References