1-Decanol, TMS derivative
- Formula: C13H30OSi
- Molecular weight: 230.4622
- IUPAC Standard InChI: InChI=1S/C13H30OSi/c1-5-6-7-8-9-10-11-12-13-14-15(2,3)4/h5-13H2,1-4H3
- IUPAC Standard InChIKey: QUGMZNIFJDARJV-UHFFFAOYSA-N
- CAS Registry Number: 18402-10-3
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Silane, (decyloxy)trimethyl-; (Decyloxy)trimethylsilane; 1-Decanol, O-TMS; Decyl alcohol, trimethylsilyl ether
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | DB-5 | DB-1 |
| Column length (m) | 20. | 15. |
| Carrier gas | He | |
| Substrate | ||
| Column diameter (mm) | 0.25 | 0.53 |
| Phase thickness (μm) | 0.25 | 1. |
| Tstart (C) | 50. | 40. |
| Tend (C) | 350. | 250. |
| Heat rate (K/min) | 5.5 | 8. |
| Initial hold (min) | 4. | |
| Final hold (min) | ||
| I | 1393.4 | 1379. |
| Reference | Richter, Komarek, et al., 1997 | Peng, 1992 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Richter, Komarek, et al., 1997
Richter, P.; Komarek, K.; Reznicková, I.,
Identification of alkylpolyethylene glycols in the residues after biodegradation of their mixtures by CGC and previous derivatization,
Folia Microbiol. (Prague), 1997, 42, 5, 517-520, https://doi.org/10.1007/BF02826565
. [all data]
Peng, 1992
Peng, C.T.,
A method for tentative identificatoin of unknown gas chromatographic peaks by retention index,
J. Radioanal. Nucl. Chem., 1992, 160, 2, 449-460, https://doi.org/10.1007/BF02037120
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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