1,3-Benzodioxole, 4-methoxy-6-(2-propenyl)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51520.Shatar S., 20053. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5MS1509.Siani, Garrido, et al., 200430. m/0.32 mm/0.25 μm, He, 70. C @ 5. min, 3. K/min; Tend: 250. C
CapillaryHP-5MS1517.Siani, Ramos, et al., 199930. m/0.32 mm/0.25 μm, He, 70. C @ 5. min, 3. K/min; Tend: 250. C
CapillaryDB-51520.da Silva, Zoghbi, et al., 199930. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-11482.Takeoka, Perrino, et al., 199660. m/0.25 mm/0.25 μm, 30. C @ 4. min, 2. K/min; Tend: 220. C
CapillaryDB-11484.Takeoka, Perrino, et al., 199660. m/0.25 mm/0.25 μm, 30. C @ 4. min, 2. K/min; Tend: 220. C
CapillaryBP-11500.Ekundayo, Laakso, et al., 1988H2, 65. C @ 2. min, 5. K/min; Column length: 50. m; Column diameter: 0.33 mm; Tend: 220. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1526.Zeng, Zhao, et al., 200730. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 80. C; Tend: 300. C
CapillaryDB-51520.Zeller and Rychlik, 200630. m/0.32 mm/0.25 μm, He, 40. C @ 1. min, 6. K/min; Tend: 230. C
CapillaryOptima 51507.Vérité, Nacer, et al., 200425. m/0.25 mm/0.25 μm, He, 3. K/min, 280. C @ 20. min; Tstart: 60. C
CapillaryDB-51516.bin Jantan, Yassin, et al., 200330. m/0.25 mm/0.25 μm, N2, 75. C @ 10. min, 3. K/min; Tend: 230. C
CapillaryHP-5MS1519.Mimica-Dukic, Kujundzic, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1523.Afsharypuor and Suleimany, 200230. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 275. C
CapillarySE-301516.bin Jantan, Basni, et al., 2001N2, 60. C @ 10. min, 3. K/min, 180. C @ 1. min; Column length: 25. m; Column diameter: 0.20 mm
CapillaryCP Sil 8 CB1522.Chevance and Farmer, 199960. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1525.2Andriamaharavo, 201430. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryHP-5MS1519.Pérez, Navarro, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 50C(4min) => 10C/min => 200C(0.5min) => 20C/min => 260C(5min)
Capillary5 % Phenyl methyl siloxane1519.Sacchetti, Maietti, et al., 200530. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min)
CapillaryBPX-51566.Elmore, Erbahadir, et al., 199750. m/0.32 mm/0.5 μm, He; Program: 0C (5min) => 40C/min => 40C (2min) => 10C/min => 280C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-FFAP2272.Zeller and Rychlik, 200630. m/0.32 mm/0.25 μm, He, 40. C @ 1. min, 6. K/min; Tend: 230. C
CapillaryCP-Wax 52CB2225.Kjeldsen, Christensen, et al., 200350. m/0.25 mm/0.2 μm, He, 32. C @ 1. min, 1. K/min; Tend: 220. C
CapillaryCP-Wax 52CB2225.Kjeldsen, Christensen, et al., 200150. m/0.25 mm/0.2 μm, 32. C @ 1. min, 1. K/min; Tend: 220. C
CapillaryCP-Wax 52CB2247.Chevance and Farmer, 199960. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryCP-Wax 52CB2262.Chevance and Farmer, 1999, 260. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryCP-Wax 52CB2262.Chevance and Farmer, 1999, 240. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDP-51516.Vijayakumar, Duraipandiyan, et al., 201230. m/0.25 mm/0.25 μm, Helium, 80. C @ 1. min, 4. K/min, 300. C @ 40. min
CapillaryDP-51516.Vijayakumar, Duraipandiyan, et al., 201230. m/0.25 mm/0.25 μm, Helium, 80. C @ 1. min, 4. K/min, 300. C @ 40. min
CapillaryDB-11492.Misharina T., 201150. m/0.32 mm/0.25 μm, Helium, 8. K/min; Tstart: 60. C; Tend: 250. C
CapillaryDB-51519.Pattiram, Lasekan, et al., 201130. m/0.32 mm/0.25 μm, Helium, 2. K/min; Tstart: 35. C; Tend: 200. C
CapillaryDB-51509.Georgiou, Koutsaviti, et al., 201030. m/0.32 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-11501.Hajimahdipoor, Samadi, et al., 201030. m/0.25 mm/0.25 μm, Helium, 50. C @ 1. min, 2.5 K/min, 265. C @ 20. min
CapillaryHP-5 MS1527.Radulovic, Blagojevic, et al., 201030. m/0.25 mm/0.25 μm, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C
CapillaryDB-11500.Xu, Tang, et al., 201030. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 4. K/min, 220. C @ 2. min
CapillaryHP-5MS1524.Males, Plazibat, et al., 200960. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 70. C; Tend: 250. C
CapillaryDB-51519.Rahimi-Nasrabadi, Gholivand, et al., 200930. m/0.25 mm/0.25 μm, Nitrogen, 40. C @ 1. min, 3. K/min, 250. C @ 10. min
CapillaryHP-5 MS1523.Zhao, Zeng, et al., 200930. m/0.25 mm/0.25 μm, Helium, 4. K/min; Tstart: 50. C; Tend: 280. C
CapillaryDB-51533.Chieng, Assim, et al., 200825. m/0.22 mm/0.25 μm, Nitrogen, 50. C @ 2. min, 6.5 K/min, 300. C @ 7. min
CapillaryHP-51519.Yassa and Akhani, 200830. m/0.25 mm/0.32 μm, Helium, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillaryCol-Elite 5MS1527.Gudaityte and Venskutonis R.P., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 30. C; Tend: 246. C
CapillaryDB-51511.Limberger, Scopel, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 300. C
CapillaryBPX-51563.Rali, Wossa, et al., 200750. m/0.22 mm/1. μm, He, 50. C @ 1. min, 4. K/min, 300. C @ 10. min
CapillaryHP-51519.Yassa and Akhani, 200730. m/0.25 mm/0.32 μm, He, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillaryHP-51565.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 μm, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryHP-5MS1518.Bozin, Mimicá-Dukic, et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51519.Champagnat, Figueredo, et al., 200625. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 5. K/min; Tend: 300. C
CapillaryDB-11475.Iranshahi, Amin, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 2.5 K/min, 265. C @ 20. min
CapillaryCP Sil 5 CB1494.Kurowska and Galazka, 200630. m/0.25 mm/0.25 μm, N2, 60. C @ 4. min, 5. K/min; Tend: 300. C
CapillaryHP-51514.Miyazawa and Kawata, 200630. m/0.32 mm/0.25 μm, Helium, 4. K/min, 240. C @ 5. min; Tstart: 40. C
CapillaryHP-11490.Valette, Fernandez, et al., 200650. m/0.2 mm/0.5 μm, He, 2. K/min, 250. C @ 40. min; Tstart: 60. C
CapillaryDB-11498.Cégiéla-Carlioz, Bessière, et al., 200525. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 3. K/min; Tend: 250. C
CapillaryHP-5MS1498.Pourmortazavi, Ghadiri, et al., 200530. m/0.25 mm/0.32 μm, He, 60. C @ 3. min, 5. K/min; Tend: 250. C
CapillaryDB-11519.bin Jantan, Ayop, et al., 200425. m/0.25 mm/0.25 μm, 60. C @ 10. min, 3. K/min, 180. C @ 10. min
CapillaryDB-51514.Tellez, Khan, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryOV-1011500.Orav, Kailas, et al., 200350. m/0.2 mm/0.5 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-11482.Velasco-Negueruela, Pérez-Alonso, et al., 200350. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 90. C; Tend: 240. C
CapillaryHP-51525.Yassa, Akhani, et al., 200330. m/0.25 mm/0.32 μm, He, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillaryRSL-2001502.Jirovetz, Buchbauer, et al., 200230. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-51523.Palmeira, Conserva, et al., 200130. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 270. C
CapillarySPB-11491.Choo, Wong, et al., 199950. m/0.2 mm/0.33 μm, 4. K/min; Tstart: 60. C; Tend: 260. C
CapillaryOV-1011478.Pateira, Nogueira, et al., 199950. m/0.25 mm/0.25 μm, He, 70. C @ 5. min, 2. K/min; Tend: 220. C
CapillaryDB-51523.Maia, Zohhbi, et al., 199830. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryOV-1011532.Zollo, Biyiti, et al., 19985. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5 MS1529.Wang, Xu, et al., 201130. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (1.5 min) 10 0C/min -> 180 0C (2 min) 6 0C/min -> 280 0C (10 min)
CapillaryDB-51515.Pontes, Silva, et al., 201030. m/0.25 mm/0.25 μm, Hydrogen; Program: 35 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 280 0C
CapillaryHP-5 MS1491.Sharifiar, Yassa, et al., 201030. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (3 min) 3 0C/min -> 160 0C (10 min) 3 0C/min -> 240 0C
CapillaryDB-11526.Xu, Tang, et al., 201030. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryOV-11483.Li, Liang, et al., 2009Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: 40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)
CapillaryDB-11493.Mendes, Trindade, et al., 200930. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)
CapillaryDB-51532.Chieng, Assim, et al., 200825. m/0.22 mm/0.25 μm, Nitrogen; Program: not specified
CapillaryRTX-51526.Zachariah, Leela, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (5 min) 5 0C/min -> 110 0C 3 0C/min -> 220 0C (5 min)
CapillaryRTX-51519.Zachariah, Leela, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryDB-51519.Nivinsliene, Butkiene, et al., 200750. m/0.32 mm/0.25 μm, Helium; Program: 60 0C (1 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C
CapillaryHP-5 MS1511.Sharififar, Mozaffarian, et al., 200730. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryHP-5MS1520.Singh, Marimuthu, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 60C => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)
CapillaryHP-5MS1528.Ansorena, Gimeno, et al., 200130. m/0.25 mm/0.25 μm, He; Program: 40C (10min) => 3C/min => 120C => 10C/min => 250C (5min)
CapillaryDB-11493.Dorman, Figueiredo, et al., 200030. m/0.25 mm/0.25 μm, H2; Program: 40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)
CapillaryDB-11493.Pedro, da Silva, et al., 199930. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 170C => 15C/min => 300C(10min)
CapillaryDB-11493.Santos, Figueiredo, et al., 199930. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 300C(10min)
CapillaryRTX-51533.Masanetz and Grosch, 199830. m/0.53 mm/1.5 μm, He; Program: 35 0C (2 min) 40 0C/min -> 60 0C (1 min) 6 0C/min -> 230 0C
CapillaryDB-11493.Figueiredo, Barroso, et al., 199730. m/0.25 mm/0.25 μm, H2; Program: 45C => 3C/min => 175C => 15C/min => 240C(10min)

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Wax2257.Lee, Umano, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min, 180. C @ 40. min; Tstart: 50. C
CapillarySupelcowax-102246.Orav, Kailas, et al., 200350. m/0.2 mm/0.25 μm, He, 2. K/min; Tstart: 70. C; Tend: 230. C
CapillaryHP-Innowax2258.Velasco-Negueruela, Pérez-Alonso, et al., 200350. m/0.2 mm/0.2 μm, He, 5. K/min; Tstart: 70. C; Tend: 190. C
CapillarySupelcowax-102256.Choo, Wong, et al., 199930. m/0.25 mm/0.25 μm, 4. K/min; Tstart: 60. C; Tend: 220. C
CapillaryTC-Wax2289.Shuichi, Masazumi, et al., 199680. C @ 5. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 240. C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryPEG-20M Innowax2286.Wang, Tian, et al., 201330. m/0.25 mm/0.25 μm, Nitrogen; Program: 50 0C (7 min) 20 0C/min -> 130 0C (1 min) 1 0C/min -> 150 0C 8 0C/min -> 190 0C (5 min)
CapillaryHP-Innowax FSC2296.Kürkçüoglu, Hüsnü Can Baser, et al., 200660. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C
CapillaryInnowax FSC2296.Kosar, Özek, et al., 200560. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryInnowax FSC2296.Kosar, Özek, et al., 200560. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryInnowax2296.Özcan, Akgül, et al., 200160. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 200C(10min) => 1C/min => 240C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Shatar S., 2005
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Notes

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