Furan, 2-pentyl-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5 MSVF-5 MSHP-5VF-5 MSVF-5 MS
Column length (m) 30.60.30.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.40.60.30.30.
Tend (C) 250.250.240.260.260.
Heat rate (K/min) 10.4.3.2.2.
Initial hold (min) 3.2.2.  
Final hold (min) 5.  28.28.
I 992.990.991.991.993.
ReferenceGoeminne, Vandendriessche, et al., 2012Srisajjalerwaja, Apichartsrangkoon, et al., 2012Kahriman, Tosun, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSRTX-1HP-5HP-5 MSHP-5
Column length (m) 30.60.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHydrogen
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.70.70.
Tend (C) 260.230.240.290.290.
Heat rate (K/min) 4.2.3.5.5.
Initial hold (min)   2.  
Final hold (min) 5.30. 10. 
I 993.981.992.993.995.
ReferenceMiyazawa, Marumoto, et al., 2011Dib, Djabou, et al., 2010Kahriman, Tosun, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1-MSDB-1DB-5 MSDB-5 MS
Column length (m) 30.60.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.30.50.40.40.
Tend (C) 290.200.220.230.250.
Heat rate (K/min) 5.2.4.6.6.
Initial hold (min)  4.2.2.2.
Final hold (min) 10.35.2.20.20.
I 990.981.977.1010.993.
ReferenceRadulovic, Dordevic, et al., 2010, 2Takeoka, Hobbs, et al., 2010Xu, Tang, et al., 2010Chen, Song, et al., 2009Chen, Song, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSVF-5HP-5 MSHP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.60.70.50.50.
Tend (C) 195.300.290.280.230.
Heat rate (K/min) 2.10.5.4.4.
Initial hold (min) 5.2.  4.
Final hold (min) 30.10.10. 10.
I 991.994.995.990.994.
ReferenceKim and Chung, 2009Li and Zhao, 2009Radulovic, Blagojevic, et al., 2009Zhao, Zeng, et al., 2009Forero, Quijano, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SLB-5MSHP-5 MSHP-5 MSVF-5MS
Column length (m) 30.10.30.30.30.
Carrier gas HeliumHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.180.250.320.25
Phase thickness (μm) 1.00.180.250.250.25
Tstart (C) 60.40.50.60.40.
Tend (C) 250.295.250.280.250.
Heat rate (K/min) 5.10.6.54.7.
Initial hold (min) 5.1.51.55. 
Final hold (min)   10.  
I 983.990.993.987.989.
ReferenceFrerot, Velluz, et al., 2008Risticevic, Carasek, et al., 2008Thakeow, Angeli, et al., 2008Capetanos, Saroglou, et al., 2007Ghiasvand, Setkova, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5 MSSPB-5HP-1
Column length (m) 60.30.30.60.50.
Carrier gas HeliumHeliumHelium He
Substrate      
Column diameter (mm) 0.320.250.250.320.2
Phase thickness (μm) 1.00.250.251.0.5
Tstart (C) 35.40.60.40.60.
Tend (C) 240.260.280.230.250.
Heat rate (K/min) 15.4.3.3.2.
Initial hold (min) 7.  5. 
Final hold (min) 10.  5.120.
I 993.987.1002.994.975.
ReferenceGogus, Ozel, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Tsokou, Georgopoulos, et al., 2007Vasta, Ratel, et al., 2007Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1DB-5DB-1DB-5
Column length (m) 50.60.60.30.30.
Carrier gas HeNitrogenHeHeHe
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (μm) 0.33  0.250.25
Tstart (C) 60.40.60.50.60.
Tend (C) 250.200.250.265.220.
Heat rate (K/min) 2.2.4.2.54.
Initial hold (min) 4.1.5.1.5.
Final hold (min) 30.9. 20. 
I 975.973.990.973.991.
ReferenceCastel, Fernandez, et al., 2006Chen, Sheu, et al., 2006Fadel, Mageed, et al., 2006Iranshahi, Amin, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-1HP-1BPX5
Column length (m) 30.30.50.50.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.20.20
Phase thickness (μm) 0.250.250.50.50.13
Tstart (C) 40.40.60.60.50.
Tend (C) 260.250.250.250.230.
Heat rate (K/min) 2.4.2.2.3.
Initial hold (min) 5.2.  2.
Final hold (min) 20.10.40.60. 
I 1001.976.980.981.990.
ReferenceSenatore, Landolfi, et al., 2006Shen X., Gao Y., et al., 2006Valette, Fernandez, et al., 2006Bendimerad and Bendiab, 2005Boustie, Rapior, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5HP-5MDN-5MDN-5CP Sil 5 CB
Column length (m) 30.60.60.60.25.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.15
Tstart (C) 40.30.40.40.50.
Tend (C) 200.260.270.270.230.
Heat rate (K/min) 5.2.4.4.3.
Initial hold (min) 8.2.4.4. 
Final hold (min) 10.28.5.5. 
I 1012.997.2991.995.981.
ReferenceKalua, Allen, et al., 2005Leffingwell and Alford, 2005van Loon, Linssen, et al., 2005van Loon, Linssen, et al., 2005Olawore, Ogunwande, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 40.40.40.60.60.
Tend (C) 260.300.250.260.240.
Heat rate (K/min) 2.4.5.5.2.
Initial hold (min) 5. 2.2. 
Final hold (min) 20.5.5.13.999.
I 1001.974.991.998.982.
ReferenceSenatore, Apostolides Arnold, et al., 2005Utsunomia, Kawata, et al., 2005N/AYayli, Yasar, et al., 2005Miyazawa, Fuhita, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-55 % Phenyl methyl siloxaneCP Sil 8 CBDB-5SPB-5
Column length (m) 50.0.30.60.60.
Carrier gas HeliumHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm)  1.0.250.251.0
Tstart (C) 60.40.50.35.30.
Tend (C) 240.250.200.280.230.
Heat rate (K/min) 2.7.10.5.3.
Initial hold (min)  10.3.2. 
Final hold (min) 999.5.2.4. 
I 982.994.989.989.992.
ReferenceMiyazawa, Fujita, et al., 2004Ramírez, Estévez, et al., 2004Wang and Guo-Y. -L., 2004Dhanda, Pegg, et al., 2003Sebastian, Viallon-Fernandez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1SPB-1HP-5DB-5RSL-200
Column length (m) 50.30.50.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (μm) 0.50.251.050.250.25
Tstart (C) 60.40.40.60.40.
Tend (C) 220.200.200.240.280.
Heat rate (K/min) 2.3.5.3.6.
Initial hold (min)  10.10. 2.
Final hold (min) 40. 5. 10.
I 973.979.997.990.987.
ReferenceValette, Fernandez, et al., 2003Vichi, Pizzale, et al., 2003Andrés, Cava, et al., 2002Flamini, Ertugrul, et al., 2002Jirovetz, Smith, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5SPB-5OV-101HP-5
Column length (m) 30.30.60.50.50.
Carrier gas HeN2HeNitrogen 
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.250.251. 0.52
Tstart (C) 60.60.40.40.35.
Tend (C) 240.220.200.200.250.
Heat rate (K/min) 3.5.3.2.2.
Initial hold (min)  10. 10.15.
Final hold (min)     45.
I 992.994.996.978.991.
ReferenceTellez, Khan, et al., 2002Campeol, Flamini, et al., 2001Poligné, Collignan, et al., 2001Tamura, Boonbumrung, et al., 2000Boylston and Viniyard, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1DB-1HP-5DB-1
Column length (m) 25.60.60. 60.
Carrier gas   He He
Substrate      
Column diameter (mm) 0.320.250.25 0.32
Phase thickness (μm)      
Tstart (C) 35.30.30.35.30.
Tend (C) 250.200.200.200.200.
Heat rate (K/min) 4.4.4.6.4.
Initial hold (min)  25.25.2.25.
Final hold (min)  20.20. 20.
I 980.977.977.994.977.
ReferenceOng, Acree, et al., 1998Buttery, Ling, et al., 1997Buttery and Ling, 1995Larsen and Frisvad, 1995Buttery, Stern, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HG-5DB-5DB-5
Column length (m) 30.30.50.60.60.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.520.25 
Tstart (C) 50.50.35.40.40.
Tend (C) 240.240.250.250.160.
Heat rate (K/min) 5.5.3.2.2.
Initial hold (min) 3.3.15.5.5.
Final hold (min)   45.  
I 975.976.993.992.995.
ReferenceShiota, 1993Shiota, 1993Drumm and Spanier, 1991Lee, Macku, et al., 1991Macku and Shibamoto, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1OV-101OV-101DB-1
Column length (m) 60.60.50.50.60.
Carrier gas HeHeNitrogenNitrogen 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm)     0.25
Tstart (C) 40.30.70.80.50.
Tend (C) 160.200.200.200.250.
Heat rate (K/min) 2.4.2.2.4.
Initial hold (min) 5.25.   
Final hold (min)  5.   
I 995.977.979.978.977.
ReferenceMacku and Shibamoto, 1991, 2Buttery, Teranishi, et al., 1990Sugisawa, Nakamura, et al., 1990Sugisawa, Nakamura, et al., 1990Flath, Matsumoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1BP-1DB-1DB-1
Column length (m) 60.25.25.50.50.
Carrier gas  NitrogenHydrogen  
Substrate      
Column diameter (mm) 0.320.330.200.320.32
Phase thickness (μm) 0.251.00   
Tstart (C) 50.30.70.0.50.
Tend (C) 250.150.180.250.250.
Heat rate (K/min) 4.5.3.3.3.
Initial hold (min)  4.5.  
Final hold (min)      
I 977.972.983.978.977.
ReferenceFlath, Matsumoto, et al., 1989Wilkins and Scholl, 1989MacLeod, MacLeod, et al., 1988Habu, Flath, et al., 1985Habu, Flath, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase OV-101SP 2100SE-30
Column length (m) 50.40.50.
Carrier gas HeHeliumHe
Substrate    
Column diameter (mm) 0.310.200.5
Phase thickness (μm)    
Tstart (C) 0.40.40.
Tend (C) 225.200.170.
Heat rate (K/min) 3.10.3.
Initial hold (min) 1. 3.
Final hold (min)    
I 977.982.978.
Referencedel Rosario, de Lumen, et al., 1984Labropoulos, Palmer, et al., 1982Heydanek and McGorrin, 1981
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References